An Improved Procedure for the Gas Chromatography–Tandem Mass Spectrometry Detection of the Globin Adduct of Sulfur Mustard
Тип публикации: Journal Article
Дата публикации: 2018-12-01
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SJR: 0.252
CiteScore: 1.9
Impact factor: 1.1
ISSN: 10619348, 16083199
Analytical Chemistry
Краткое описание
Features of the electron and chemical ionization mass spectra of derivatives of N-[2-[(hydroxyethyl)thio]ethyl]-DL-valine (НЕТЕ-Val)—a biomarker of sulfur mustard—recorded by GC–MS and GC–MS/MS are studied. The retention indices of the studied derivatives were measured. An optimized procedure of the GC–MS/MS (MRM mode) identification of НЕТЕ-Val was tested in the analysis of donor blood samples in vitro exposed to sulfur mustard. The linear range of the detector was from 10 to 100 ng mL–1, and the limit of detection for sulfur mustard was 10 ng mL–1.
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Koryagina N. L. et al. An Improved Procedure for the Gas Chromatography–Tandem Mass Spectrometry Detection of the Globin Adduct of Sulfur Mustard // Journal of Analytical Chemistry. 2018. Vol. 73. No. 13. pp. 1269-1274.
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Koryagina N. L., Shachneva M. D., Ukolov A. I., Saveleva E. I., Khlebnikova N. S., Radilov A. S. An Improved Procedure for the Gas Chromatography–Tandem Mass Spectrometry Detection of the Globin Adduct of Sulfur Mustard // Journal of Analytical Chemistry. 2018. Vol. 73. No. 13. pp. 1269-1274.
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TY - JOUR
DO - 10.1134/s1061934818130087
UR - https://doi.org/10.1134/s1061934818130087
TI - An Improved Procedure for the Gas Chromatography–Tandem Mass Spectrometry Detection of the Globin Adduct of Sulfur Mustard
T2 - Journal of Analytical Chemistry
AU - Koryagina, N L
AU - Shachneva, M D
AU - Ukolov, A I
AU - Saveleva, E I
AU - Khlebnikova, N S
AU - Radilov, A S
PY - 2018
DA - 2018/12/01
PB - Pleiades Publishing
SP - 1269-1274
IS - 13
VL - 73
SN - 1061-9348
SN - 1608-3199
ER -
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@article{2018_Koryagina,
author = {N L Koryagina and M D Shachneva and A I Ukolov and E I Saveleva and N S Khlebnikova and A S Radilov},
title = {An Improved Procedure for the Gas Chromatography–Tandem Mass Spectrometry Detection of the Globin Adduct of Sulfur Mustard},
journal = {Journal of Analytical Chemistry},
year = {2018},
volume = {73},
publisher = {Pleiades Publishing},
month = {dec},
url = {https://doi.org/10.1134/s1061934818130087},
number = {13},
pages = {1269--1274},
doi = {10.1134/s1061934818130087}
}
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Koryagina, N. L., et al. “An Improved Procedure for the Gas Chromatography–Tandem Mass Spectrometry Detection of the Globin Adduct of Sulfur Mustard.” Journal of Analytical Chemistry, vol. 73, no. 13, Dec. 2018, pp. 1269-1274. https://doi.org/10.1134/s1061934818130087.