Study of the Aniline and Acetone Condensation Reaction under Electrospray Ionization Conditions
D O Kuleshov
1
,
D M Mazur
2
,
I A Gromov
1, 3
,
E N Alekseyuk
4
,
N. R. Gall
1, 3
,
O V Polyakova
2
,
A. T. Lebedev
2
,
L.N. Gall
1
Publication type: Journal Article
Publication date: 2020-12-20
scimago Q3
wos Q4
SJR: 0.252
CiteScore: 1.9
Impact factor: 1.1
ISSN: 10619348, 16083199
Analytical Chemistry
Abstract
The present paper deals with the study of condensation reaction of aniline with acetone under electrospray ionization (ESI) conditions . An experimental setup is described for conducting reactions under ESI conditions with a possibility of the accumulation of reaction products. The aniline and acetone condensation products were analyzed by gas chromatography–mass spectrometry. Spraying this mixture with high concentration of formic acid, results in the formation of N-phenylformamide, N,N'-diphenylmethaneimidamide, and 1,2-dihydro-2,2,4-trimethylquinoline; the last one is the only product of the reaction of aniline with acetone. Thus, the Schiff base formation reaction radically changes its direction. The results obtained using the proposed experimental setup open up new prospects both for studying chemical reactions in charged microdroplets and for the use of ESI as a preparative method for the synthesis of organic compounds.
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Total citations:
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Citations from 2024:
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(66%)
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Kuleshov D. O. et al. Study of the Aniline and Acetone Condensation Reaction under Electrospray Ionization Conditions // Journal of Analytical Chemistry. 2020. Vol. 75. No. 13. pp. 1647-1652.
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Kuleshov D. O., Mazur D. M., Gromov I. A., Alekseyuk E. N., Gall N. R., Polyakova O. V., Lebedev A. T., Gall L. Study of the Aniline and Acetone Condensation Reaction under Electrospray Ionization Conditions // Journal of Analytical Chemistry. 2020. Vol. 75. No. 13. pp. 1647-1652.
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RIS
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TY - JOUR
DO - 10.1134/S1061934820130067
UR - https://doi.org/10.1134/S1061934820130067
TI - Study of the Aniline and Acetone Condensation Reaction under Electrospray Ionization Conditions
T2 - Journal of Analytical Chemistry
AU - Kuleshov, D O
AU - Mazur, D M
AU - Gromov, I A
AU - Alekseyuk, E N
AU - Gall, N. R.
AU - Polyakova, O V
AU - Lebedev, A. T.
AU - Gall, L.N.
PY - 2020
DA - 2020/12/20
PB - Pleiades Publishing
SP - 1647-1652
IS - 13
VL - 75
SN - 1061-9348
SN - 1608-3199
ER -
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BibTex (up to 50 authors)
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@article{2020_Kuleshov,
author = {D O Kuleshov and D M Mazur and I A Gromov and E N Alekseyuk and N. R. Gall and O V Polyakova and A. T. Lebedev and L.N. Gall},
title = {Study of the Aniline and Acetone Condensation Reaction under Electrospray Ionization Conditions},
journal = {Journal of Analytical Chemistry},
year = {2020},
volume = {75},
publisher = {Pleiades Publishing},
month = {dec},
url = {https://doi.org/10.1134/S1061934820130067},
number = {13},
pages = {1647--1652},
doi = {10.1134/S1061934820130067}
}
Cite this
MLA
Copy
Kuleshov, D. O., et al. “Study of the Aniline and Acetone Condensation Reaction under Electrospray Ionization Conditions.” Journal of Analytical Chemistry, vol. 75, no. 13, Dec. 2020, pp. 1647-1652. https://doi.org/10.1134/S1061934820130067.
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