Synthesis and physicochemical characterization of a porous coordination polymer of Sn-Cu xylarate: The structure of [Sn4 Cu 8.5 (HL)2 (L)4 O2 (OH)(H 2 O)12.5 ] · 17.2H2 O
Publication type: Journal Article
Publication date: 2013-03-21
scimago Q4
wos Q4
SJR: 0.145
CiteScore: 0.8
Impact factor: 0.5
ISSN: 10637745, 1562689X
General Chemistry
Condensed Matter Physics
General Materials Science
Abstract
A porous coordination polymer of Sn-Cu xylarate [Sn4Cu8.5(HL)2(L)4O2(OH)(H2O)12.5] · 17.2H2O (H5L is xylaric acid) is synthesized for the first time and characterized by chemical analysis, IR spectroscopy, and X-ray diffraction. Centrosymmetric heterometallic fragments [Sn4Cu6(HL)2(L)4O2(H2O)6] (A) including copper Cu1–3 and tin Sn1,2 atoms are distinguished in the structure. The Cu4(OH)0.5(H2O)2.5 bridges connect A units into chains running along the c axis, and the Cu5(OH)(H2O) bridges connect A fragments into layers perpendicular to the c axis. The Cu4,5 atoms form a framework whose voids accommodate the crystallization water molecules.
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Sergienko V. S. et al. Synthesis and physicochemical characterization of a porous coordination polymer of Sn-Cu xylarate: The structure of [Sn4Cu 8.5(HL)2(L)4O2(OH)(H 2O)12.5] · 17.2H2O // Crystallography Reports. 2013. Vol. 58. No. 2. pp. 241-246.
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Sergienko V. S., Chebanenko E. A., Martsinko E. É., Martsinko E. E., Ilyukhin A. B., Seifullina I. I. Synthesis and physicochemical characterization of a porous coordination polymer of Sn-Cu xylarate: The structure of [Sn4Cu 8.5(HL)2(L)4O2(OH)(H 2O)12.5] · 17.2H2O // Crystallography Reports. 2013. Vol. 58. No. 2. pp. 241-246.
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TY - JOUR
DO - 10.1134/S1063774513020247
UR - http://link.springer.com/10.1134/S1063774513020247
TI - Synthesis and physicochemical characterization of a porous coordination polymer of Sn-Cu xylarate: The structure of [Sn4Cu 8.5(HL)2(L)4O2(OH)(H 2O)12.5] · 17.2H2O
T2 - Crystallography Reports
AU - Sergienko, V S
AU - Chebanenko, E A
AU - Martsinko, E É
AU - Martsinko, E. E.
AU - Ilyukhin, A. B.
AU - Seifullina, I I
PY - 2013
DA - 2013/03/21
PB - Pleiades Publishing
SP - 241-246
IS - 2
VL - 58
SN - 1063-7745
SN - 1562-689X
ER -
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@article{2013_Sergienko,
author = {V S Sergienko and E A Chebanenko and E É Martsinko and E. E. Martsinko and A. B. Ilyukhin and I I Seifullina},
title = {Synthesis and physicochemical characterization of a porous coordination polymer of Sn-Cu xylarate: The structure of [Sn4Cu 8.5(HL)2(L)4O2(OH)(H 2O)12.5] · 17.2H2O},
journal = {Crystallography Reports},
year = {2013},
volume = {58},
publisher = {Pleiades Publishing},
month = {mar},
url = {http://link.springer.com/10.1134/S1063774513020247},
number = {2},
pages = {241--246},
doi = {10.1134/S1063774513020247}
}
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MLA
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Sergienko, V. S., et al. “Synthesis and physicochemical characterization of a porous coordination polymer of Sn-Cu xylarate: The structure of [Sn4Cu 8.5(HL)2(L)4O2(OH)(H 2O)12.5] · 17.2H2O.” Crystallography Reports, vol. 58, no. 2, Mar. 2013, pp. 241-246. http://link.springer.com/10.1134/S1063774513020247.