Synthesis and the crystal and molecular structure of the germanium(IV) complex with propylene-1,3-diaminetetraacetic acid [Ge(Pdta)]
Publication type: Journal Article
Publication date: 2015-09-14
scimago Q4
wos Q4
SJR: 0.145
CiteScore: 0.8
Impact factor: 0.5
ISSN: 10637745, 1562689X
General Chemistry
Condensed Matter Physics
General Materials Science
Abstract
The germanium(IV) complex with propylene-1,3-diaminetetraacetic acid (H4Pdta) is studied by elemental analysis, X-ray diffraction, thermogravimetry, and IR spectroscopy. The X-ray diffraction study reveals two crystallographically independent [Ge(Pdta)] molecules of similar structure. Both Ge atoms are octahedrally coordinated by four O atoms and two N atoms (at the cis positions) of the hexadentate pentachelate Pdta4– ligand. An extended system of weak С—Н···О hydrogen bonds connects complex molecules into a supramolecular 3D framework.
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Sergienko V. S. et al. Synthesis and the crystal and molecular structure of the germanium(IV) complex with propylene-1,3-diaminetetraacetic acid [Ge(Pdta)] // Crystallography Reports. 2015. Vol. 60. No. 5. pp. 677-681.
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Sergienko V. S., Martsinko E. É., Seifullina I. I., Churakov A., Chebanenko E. A. Synthesis and the crystal and molecular structure of the germanium(IV) complex with propylene-1,3-diaminetetraacetic acid [Ge(Pdta)] // Crystallography Reports. 2015. Vol. 60. No. 5. pp. 677-681.
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TY - JOUR
DO - 10.1134/S1063774515040197
UR - http://link.springer.com/10.1134/S1063774515040197
TI - Synthesis and the crystal and molecular structure of the germanium(IV) complex with propylene-1,3-diaminetetraacetic acid [Ge(Pdta)]
T2 - Crystallography Reports
AU - Sergienko, V S
AU - Martsinko, E É
AU - Seifullina, I I
AU - Churakov, A.V.
AU - Chebanenko, E A
PY - 2015
DA - 2015/09/14
PB - Pleiades Publishing
SP - 677-681
IS - 5
VL - 60
SN - 1063-7745
SN - 1562-689X
ER -
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@article{2015_Sergienko,
author = {V S Sergienko and E É Martsinko and I I Seifullina and A.V. Churakov and E A Chebanenko},
title = {Synthesis and the crystal and molecular structure of the germanium(IV) complex with propylene-1,3-diaminetetraacetic acid [Ge(Pdta)]},
journal = {Crystallography Reports},
year = {2015},
volume = {60},
publisher = {Pleiades Publishing},
month = {sep},
url = {http://link.springer.com/10.1134/S1063774515040197},
number = {5},
pages = {677--681},
doi = {10.1134/S1063774515040197}
}
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Sergienko, V. S., et al. “Synthesis and the crystal and molecular structure of the germanium(IV) complex with propylene-1,3-diaminetetraacetic acid [Ge(Pdta)].” Crystallography Reports, vol. 60, no. 5, Sep. 2015, pp. 677-681. http://link.springer.com/10.1134/S1063774515040197.