X-Ray Diffraction and Thermographic Study of Mesomorphic 4-Acylphenyl 4'-Nonyloxybenzoate CH3C(O)C6H4-OC(O)-C6H4-OC9H19
Publication type: Journal Article
Publication date: 2020-05-27
scimago Q4
wos Q4
SJR: 0.145
CiteScore: 0.8
Impact factor: 0.5
ISSN: 10637745, 1562689X
General Chemistry
Condensed Matter Physics
General Materials Science
Abstract
Abstract The structure and thermal properties of mesomorphic phenyl benzoate CH 3 –C(O)–C 6 H 4 –OC(O)–C 6 H 4 –OC 9 H 19 ( I ) were studied by differential scanning calorimetry (DSC) and X-ray diffraction. The crystal packing of I is typical of mesomorphic crystals. It consists of alternating loosely packed aliphatic and closely packed aromatic regions, the latter regions being stabilized by weak directional C–H···π interactions. According to the DSC data, compound I does not form a mesophase upon melting. The latter was observed only upon cooling of the isotropic melt. The lack of enantiotropic mesomorphism in the crystal of I is attributed to the fact that C–H···π non-covalent interactions, which could ensure the structuring of the melt, are broken at the melting point.
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Kuz'mina L. G. et al. X-Ray Diffraction and Thermographic Study of Mesomorphic 4-Acylphenyl 4'-Nonyloxybenzoate CH3C(O)C6H4-OC(O)-C6H4-OC9H19 // Crystallography Reports. 2020. Vol. 65. No. 3. pp. 444-448.
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Kuz'mina L. G., KONSTANTINOV I. I., Kalle P., Navasardyan M. A. X-Ray Diffraction and Thermographic Study of Mesomorphic 4-Acylphenyl 4'-Nonyloxybenzoate CH3C(O)C6H4-OC(O)-C6H4-OC9H19 // Crystallography Reports. 2020. Vol. 65. No. 3. pp. 444-448.
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TY - JOUR
DO - 10.1134/S1063774520030190
UR - https://doi.org/10.1134/S1063774520030190
TI - X-Ray Diffraction and Thermographic Study of Mesomorphic 4-Acylphenyl 4'-Nonyloxybenzoate CH3C(O)C6H4-OC(O)-C6H4-OC9H19
T2 - Crystallography Reports
AU - Kuz'mina, L. G.
AU - KONSTANTINOV, I. I.
AU - Kalle, P
AU - Navasardyan, M. A.
PY - 2020
DA - 2020/05/27
PB - Pleiades Publishing
SP - 444-448
IS - 3
VL - 65
SN - 1063-7745
SN - 1562-689X
ER -
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@article{2020_Kuz'mina,
author = {L. G. Kuz'mina and I. I. KONSTANTINOV and P Kalle and M. A. Navasardyan},
title = {X-Ray Diffraction and Thermographic Study of Mesomorphic 4-Acylphenyl 4'-Nonyloxybenzoate CH3C(O)C6H4-OC(O)-C6H4-OC9H19},
journal = {Crystallography Reports},
year = {2020},
volume = {65},
publisher = {Pleiades Publishing},
month = {may},
url = {https://doi.org/10.1134/S1063774520030190},
number = {3},
pages = {444--448},
doi = {10.1134/S1063774520030190}
}
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Kuz'mina, L. G., et al. “X-Ray Diffraction and Thermographic Study of Mesomorphic 4-Acylphenyl 4'-Nonyloxybenzoate CH3C(O)C6H4-OC(O)-C6H4-OC9H19.” Crystallography Reports, vol. 65, no. 3, May. 2020, pp. 444-448. https://doi.org/10.1134/S1063774520030190.