,
volume 34
,
issue 8
,
pages 584-593
Synthesis, structural and multinuclear natural abundance (13C, 31P, 195Pt) CP/MAS NMR studies of crystalline O,O′-dialkyldithiophosphate platinum(II) complexes
Publication type: Journal Article
Publication date: 2008-08-07
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
Platinum(II) O,O′-dicyclohexyl dithiophosphate [Pt{S2P(O-cyclo-C6H11)2}2] (I) and platinum(II) O,O′-diisopropyl dithiophosphate [Pt{S2P(O-iso-C3H7)2}2] (II) complexes were obtained and studied by solidstate 13C, 31P, and 195Pt CP/MAS NMR spectroscopy. The dithiophosphate (Dtph) ligands in molecular structure I were found to be coordinated by platinum in S,S′-bidentate fashion to form the planar chromophore [PtS4] (single-crystal X-ray diffraction data). For complex II, a new α-form (α-II) was obtained and identified by 31P MAS NMR spectroscopy. The 31P chemical shift anisotropy δaniso and the asymmetry parameter η of the 31P chemical shift tensor were calculated from the whole MAS spectra.
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A.V. I. et al. Synthesis, structural and multinuclear natural abundance (13C, 31P, 195Pt) CP/MAS NMR studies of crystalline O,O′-dialkyldithiophosphate platinum(II) complexes // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2008. Vol. 34. No. 8. pp. 584-593.
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A.V. I., Lutsenko I. A., M. A. I., Gerasimenko A. V., Antzutkin O. N. Synthesis, structural and multinuclear natural abundance (13C, 31P, 195Pt) CP/MAS NMR studies of crystalline O,O′-dialkyldithiophosphate platinum(II) complexes // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2008. Vol. 34. No. 8. pp. 584-593.
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RIS
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TY - JOUR
DO - 10.1134/S1070328408080058
UR - https://doi.org/10.1134/S1070328408080058
TI - Synthesis, structural and multinuclear natural abundance (13C, 31P, 195Pt) CP/MAS NMR studies of crystalline O,O′-dialkyldithiophosphate platinum(II) complexes
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - A.V., Ivanov
AU - Lutsenko, I A
AU - M. A., Ivanov
AU - Gerasimenko, A V
AU - Antzutkin, O N
PY - 2008
DA - 2008/08/07
PB - Pleiades Publishing
SP - 584-593
IS - 8
VL - 34
SN - 1070-3284
SN - 1608-3318
ER -
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BibTex (up to 50 authors)
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@article{2008_A.V.,
author = {Ivanov A.V. and I A Lutsenko and Ivanov M. A. and A V Gerasimenko and O N Antzutkin},
title = {Synthesis, structural and multinuclear natural abundance (13C, 31P, 195Pt) CP/MAS NMR studies of crystalline O,O′-dialkyldithiophosphate platinum(II) complexes},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2008},
volume = {34},
publisher = {Pleiades Publishing},
month = {aug},
url = {https://doi.org/10.1134/S1070328408080058},
number = {8},
pages = {584--593},
doi = {10.1134/S1070328408080058}
}
Cite this
MLA
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A.V., Ivanov, et al. “Synthesis, structural and multinuclear natural abundance (13C, 31P, 195Pt) CP/MAS NMR studies of crystalline O,O′-dialkyldithiophosphate platinum(II) complexes.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 34, no. 8, Aug. 2008, pp. 584-593. https://doi.org/10.1134/S1070328408080058.
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