,
volume 39
,
issue 11
,
pages 751-757
Strategy for the synthesis of Di- and polymer tartratogermanates with single-charge cations. Crystal structures of K2[Ge 2(OH)2(μ-Tart)2] · 4.5H2O and (NH4)2n [Ge2(μ-O)(μ-Tart) 2] n · nMeCN · nH2O
L Kh Minacheva
1
,
I I Seifullina
2
,
A. B. Ilyukhin
1
,
E É Martsinko
2
,
V S Sergienko
1
,
E A Chebanenko
2
,
1
2
Odessa National University, Odessa, Ukraine
|
Publication type: Journal Article
Publication date: 2013-11-06
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
Tartratogermanates of alkaline metals and ammonium are synthesized for the first time using different solvents (water, acetonitrile) and starting reagents (GeO2 and GeCl4): dimeric Kat2[Ge2(OH)2(μ-Tart)2] · 4.5H2O (H4Tart is D-tartaric acid, Kat = Na (I) and K (II)) and polymer (NH4)2n[Ge2(μ-O)(μ-Tart)2]n · nCH3CN · nH2O (III). The complexes are characterized by elemental analysis, IR spectroscopy, and X-ray diffraction analysis. The structure of complex II contains binuclear isolated [Ge2(OH)2(μ-Tart)2]2-complexes. In complex III, the oxo ligands join the binuclear fragments into polymer chains.
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Minacheva L. Kh. et al. Strategy for the synthesis of Di- and polymer tartratogermanates with single-charge cations. Crystal structures of K2[Ge 2(OH)2(μ-Tart)2] · 4.5H2O and (NH4)2n [Ge2(μ-O)(μ-Tart) 2] n · nMeCN · nH2O // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2013. Vol. 39. No. 11. pp. 751-757.
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Minacheva L. Kh., Seifullina I. I., Ilyukhin A. B., Martsinko E. É., Sergienko V. S., Chebanenko E. A., Churakov A. Strategy for the synthesis of Di- and polymer tartratogermanates with single-charge cations. Crystal structures of K2[Ge 2(OH)2(μ-Tart)2] · 4.5H2O and (NH4)2n [Ge2(μ-O)(μ-Tart) 2] n · nMeCN · nH2O // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2013. Vol. 39. No. 11. pp. 751-757.
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TY - JOUR
DO - 10.1134/S1070328413110043
UR - http://link.springer.com/10.1134/S1070328413110043
TI - Strategy for the synthesis of Di- and polymer tartratogermanates with single-charge cations. Crystal structures of K2[Ge 2(OH)2(μ-Tart)2] · 4.5H2O and (NH4)2n [Ge2(μ-O)(μ-Tart) 2] n · nMeCN · nH2O
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Minacheva, L Kh
AU - Seifullina, I I
AU - Ilyukhin, A. B.
AU - Martsinko, E É
AU - Sergienko, V S
AU - Chebanenko, E A
AU - Churakov, A.V.
PY - 2013
DA - 2013/11/06
PB - Pleiades Publishing
SP - 751-757
IS - 11
VL - 39
SN - 1070-3284
SN - 1608-3318
ER -
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BibTex (up to 50 authors)
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@article{2013_Minacheva,
author = {L Kh Minacheva and I I Seifullina and A. B. Ilyukhin and E É Martsinko and V S Sergienko and E A Chebanenko and A.V. Churakov},
title = {Strategy for the synthesis of Di- and polymer tartratogermanates with single-charge cations. Crystal structures of K2[Ge 2(OH)2(μ-Tart)2] · 4.5H2O and (NH4)2n [Ge2(μ-O)(μ-Tart) 2] n · nMeCN · nH2O},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2013},
volume = {39},
publisher = {Pleiades Publishing},
month = {nov},
url = {http://link.springer.com/10.1134/S1070328413110043},
number = {11},
pages = {751--757},
doi = {10.1134/S1070328413110043}
}
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Minacheva, L. Kh., et al. “Strategy for the synthesis of Di- and polymer tartratogermanates with single-charge cations. Crystal structures of K2[Ge 2(OH)2(μ-Tart)2] · 4.5H2O and (NH4)2n [Ge2(μ-O)(μ-Tart) 2] n · nMeCN · nH2O.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 39, no. 11, Nov. 2013, pp. 751-757. http://link.springer.com/10.1134/S1070328413110043.