,
volume 40
,
issue 2
,
pages 77-83
Synthesis and molecular structures of cymantrenecarboxylate derivatives of titanium(Iv) and vanadium(III). cyclopentadienyl complexes and of copper(II) and manganese(II) lutidine complexes
Publication type: Journal Article
Publication date: 2014-02-11
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
The reactions of dimethyltitanocene borohydride and vanadocene with cymantrenecarboxylic acid CymCOOH gave the monomer (C5H4Me)2Ti(OOCCym)2 (I) and dimer (C5H5)V(OOCCym)4V(C5H5) (II), respectively. Treatment of Cu(II) cymantrenylcarboxylate with excess lutidine gives the monomer (C7H9N)2Cu(COOCym)2 (III). The reaction of lutidine with a mixture of Cu(II) and Mn(II) bis-cymantrenecarboxylates affords the heterometallic trinuclear complex (C7H9N)Cu(OOCCym)3Mn(OOCCym)3Cu(C7H9N) (IV). The structures of I–IV were established by X-ray diffraction. In I and III, the cymantrenecarboxylate groups are terminal and in II and IV, they are bridging, which is also manifested as characteristic OCO stretching bands in the IR spectra.
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Shapovalov S. S. et al. Synthesis and molecular structures of cymantrenecarboxylate derivatives of titanium(Iv) and vanadium(III). cyclopentadienyl complexes and of copper(II) and manganese(II) lutidine complexes // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2014. Vol. 40. No. 2. pp. 77-83.
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Shapovalov S. S., Pasynskii A. A., Skabitskii I. V., Krishtop T. A., Dobrokhotova Z. V. Synthesis and molecular structures of cymantrenecarboxylate derivatives of titanium(Iv) and vanadium(III). cyclopentadienyl complexes and of copper(II) and manganese(II) lutidine complexes // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2014. Vol. 40. No. 2. pp. 77-83.
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TY - JOUR
DO - 10.1134/S1070328414020092
UR - https://doi.org/10.1134/S1070328414020092
TI - Synthesis and molecular structures of cymantrenecarboxylate derivatives of titanium(Iv) and vanadium(III). cyclopentadienyl complexes and of copper(II) and manganese(II) lutidine complexes
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Shapovalov, S S
AU - Pasynskii, A A
AU - Skabitskii, I V
AU - Krishtop, T A
AU - Dobrokhotova, Zh V
PY - 2014
DA - 2014/02/11
PB - Pleiades Publishing
SP - 77-83
IS - 2
VL - 40
SN - 1070-3284
SN - 1608-3318
ER -
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BibTex (up to 50 authors)
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@article{2014_Shapovalov,
author = {S S Shapovalov and A A Pasynskii and I V Skabitskii and T A Krishtop and Zh V Dobrokhotova},
title = {Synthesis and molecular structures of cymantrenecarboxylate derivatives of titanium(Iv) and vanadium(III). cyclopentadienyl complexes and of copper(II) and manganese(II) lutidine complexes},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2014},
volume = {40},
publisher = {Pleiades Publishing},
month = {feb},
url = {https://doi.org/10.1134/S1070328414020092},
number = {2},
pages = {77--83},
doi = {10.1134/S1070328414020092}
}
Cite this
MLA
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Shapovalov, S. S., et al. “Synthesis and molecular structures of cymantrenecarboxylate derivatives of titanium(Iv) and vanadium(III). cyclopentadienyl complexes and of copper(II) and manganese(II) lutidine complexes.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 40, no. 2, Feb. 2014, pp. 77-83. https://doi.org/10.1134/S1070328414020092.