,
volume 40
,
issue 12
,
pages 871-874
Binuclear complex of silver(I) perrhenate with phthalazine: Synthesis, crystal structure, and luminescence properties
Publication type: Journal Article
Publication date: 2014-12-02
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
Silver compound Ag2(Phtz)4](ReO4)2 (I) (Phtz is phthalazine, C8H6N2) is synthesized, and its crystal structure is determined. The crystals are triclinic: space group $$P\bar 1$$, a = 9.651(2), b = 9.655(2), c = 10.884(2) Å, α = 115.752(2)°, β = 94.582(2)°, γ = 106.000(2)°, V = 854.3(2) Å3, Z = 1, ρcalcd = 2.404 g/cm3. The Ag atom forms a triangular coordination mode (Ag(1)-N(11) 2.34(2), Ag(1)-N(12À) 2.24(2), and Ag(1)-N(21) 2.28(1) Å) by the nitrogen atoms of one monodentate and two bridging phthalazine molecules. Their interaction results in the formation of an almost planar centrosymmetric binuclear cationic complex [Ag2(Phtz)4]2+ (Ag(1)⋯Ag(1A) 3.452(7) Å). The oxygen atoms of the ReO4− anion are randomly disordered over three positions each. The luminescence spectrum contains an emission band in the green region.
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Kokunov Yu. V. et al. Binuclear complex of silver(I) perrhenate with phthalazine: Synthesis, crystal structure, and luminescence properties // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2014. Vol. 40. No. 12. pp. 871-874.
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Kokunov Yu. V., Kovalev V. V., Gorbunova Yu. E., Churakov A., Kozyukhin S. A. Binuclear complex of silver(I) perrhenate with phthalazine: Synthesis, crystal structure, and luminescence properties // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2014. Vol. 40. No. 12. pp. 871-874.
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TY - JOUR
DO - 10.1134/S1070328414120070
UR - http://link.springer.com/10.1134/S1070328414120070
TI - Binuclear complex of silver(I) perrhenate with phthalazine: Synthesis, crystal structure, and luminescence properties
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Kokunov, Yu V
AU - Kovalev, V V
AU - Gorbunova, Yu E
AU - Churakov, A.V.
AU - Kozyukhin, S A
PY - 2014
DA - 2014/12/02
PB - Pleiades Publishing
SP - 871-874
IS - 12
VL - 40
SN - 1070-3284
SN - 1608-3318
ER -
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@article{2014_Kokunov,
author = {Yu V Kokunov and V V Kovalev and Yu E Gorbunova and A.V. Churakov and S A Kozyukhin},
title = {Binuclear complex of silver(I) perrhenate with phthalazine: Synthesis, crystal structure, and luminescence properties},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2014},
volume = {40},
publisher = {Pleiades Publishing},
month = {dec},
url = {http://link.springer.com/10.1134/S1070328414120070},
number = {12},
pages = {871--874},
doi = {10.1134/S1070328414120070}
}
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Kokunov, Yu. V., et al. “Binuclear complex of silver(I) perrhenate with phthalazine: Synthesis, crystal structure, and luminescence properties.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 40, no. 12, Dec. 2014, pp. 871-874. http://link.springer.com/10.1134/S1070328414120070.
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