New paramagnetic tin(IV) complexes based on o-iminoquinone ligands: Synthesis and thermal transformation

Publication typeJournal Article
Publication date2015-06-24
scimago Q4
wos Q4
SJR0.189
CiteScore1.7
Impact factor1.1
ISSN10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
A series of new paramagnetic tin(IV) complexes based on sterically hindered o-iminobenzoquinones (R)ImQ differed in fragments (R) in the N-aryl fragment is synthesized. The thermal transformation of the tin(IV) complex, (iso-Pr)ImSQSn(tert-Bu)2Cl ((iso-Pr)ImSQ is the radical anion of 4,6-di-tert-butyl-N-(2,6-di-iso-propylphenyl)-o-iminobenzoquinone), is studied. The thermal transformation of the paramagnetic complex in nonane results in the formation of a new tin(II) bis(aminophenolate) derivative. The synthesized complexes and the thermolysis product are characterized by EPR, IR, and 1H, 13C, and 119Sn NMR spectroscopy and elemental analysis. The structures of the (tert-Bu)ImSQSn(tert-Bu)2Cl complex and the thermal decomposition product, {(iso-Pr)AmPh}2Sn ((iso-Pr)AmPh is 2-(2,6-di-iso-propylphenyl)amino-4,6-di-tert-butylphenolate), are determined by X-ray diffraction analysis.
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Piskunov A. V. et al. New paramagnetic tin(IV) complexes based on o-iminoquinone ligands: Synthesis and thermal transformation // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2015. Vol. 41. No. 7. pp. 428-435.
GOST all authors (up to 50) Copy
Piskunov A. V., Chegerev M. G., Vaganova L. B., Fukin G. K. New paramagnetic tin(IV) complexes based on o-iminoquinone ligands: Synthesis and thermal transformation // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2015. Vol. 41. No. 7. pp. 428-435.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1134/S1070328415070076
UR - https://doi.org/10.1134/S1070328415070076
TI - New paramagnetic tin(IV) complexes based on o-iminoquinone ligands: Synthesis and thermal transformation
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Piskunov, A. V.
AU - Chegerev, M G
AU - Vaganova, L B
AU - Fukin, G. K.
PY - 2015
DA - 2015/06/24
PB - Pleiades Publishing
SP - 428-435
IS - 7
VL - 41
SN - 1070-3284
SN - 1608-3318
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2015_Piskunov,
author = {A. V. Piskunov and M G Chegerev and L B Vaganova and G. K. Fukin},
title = {New paramagnetic tin(IV) complexes based on o-iminoquinone ligands: Synthesis and thermal transformation},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2015},
volume = {41},
publisher = {Pleiades Publishing},
month = {jun},
url = {https://doi.org/10.1134/S1070328415070076},
number = {7},
pages = {428--435},
doi = {10.1134/S1070328415070076}
}
MLA
Cite this
MLA Copy
Piskunov, A. V., et al. “New paramagnetic tin(IV) complexes based on o-iminoquinone ligands: Synthesis and thermal transformation.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 41, no. 7, Jun. 2015, pp. 428-435. https://doi.org/10.1134/S1070328415070076.