,
volume 42
,
issue 9
,
pages 608-613
Heterometallic palladium-copper and palladium-nickel complexes with pivalate bridges
Publication type: Journal Article
Publication date: 2016-09-15
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
Reactions of (α-Pic)2Pd(OOCCMe3)2 (I) with dinuclear copper pivalate dihydrate and polymeric nickel bispivalate afforded the complexes (α-Pic)2Pd(μ-OOCCMe3)2Cu2(μ-OOCCMe3)4 (II) and Pd(μ- OOCCMe3)4Ni(α-Pic) (III), respectively, which were structurally characterized. The lantern dimers in complex II show no Cu···Cu bonds (Cu···Cu, 2.671(3) Å) and are united to form chains through the axial bridging pivalate groups inherited from palladium monomer I. In contrast, complex III features heterometallic palladium- nickel lanterns in which the Ni atom has an axial α-picoline ligand, while the Pd atom has no axial ligand; instead, a short Pd–Ni bond is formed (2.4976(3) Å). For triplet-state complex III and its zinc analog Pd(μ-OOCCMe3)4Zn(α-Pic) (IV), quantum chemical calculations and topological analysis of the electron density were performed.
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Pasynskii A. A. et al. Heterometallic palladium-copper and palladium-nickel complexes with pivalate bridges // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2016. Vol. 42. No. 9. pp. 608-613.
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Pasynskii A. A., Shapovalov S. S., Skabitskii I. V., Tikhonova O. G. Heterometallic palladium-copper and palladium-nickel complexes with pivalate bridges // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2016. Vol. 42. No. 9. pp. 608-613.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1134/S1070328416090062
UR - https://doi.org/10.1134/S1070328416090062
TI - Heterometallic palladium-copper and palladium-nickel complexes with pivalate bridges
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Pasynskii, A A
AU - Shapovalov, S S
AU - Skabitskii, I V
AU - Tikhonova, O G
PY - 2016
DA - 2016/09/15
PB - Pleiades Publishing
SP - 608-613
IS - 9
VL - 42
SN - 1070-3284
SN - 1608-3318
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2016_Pasynskii,
author = {A A Pasynskii and S S Shapovalov and I V Skabitskii and O G Tikhonova},
title = {Heterometallic palladium-copper and palladium-nickel complexes with pivalate bridges},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2016},
volume = {42},
publisher = {Pleiades Publishing},
month = {sep},
url = {https://doi.org/10.1134/S1070328416090062},
number = {9},
pages = {608--613},
doi = {10.1134/S1070328416090062}
}
Cite this
MLA
Copy
Pasynskii, A. A., et al. “Heterometallic palladium-copper and palladium-nickel complexes with pivalate bridges.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 42, no. 9, Sep. 2016, pp. 608-613. https://doi.org/10.1134/S1070328416090062.