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том 45
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издание 2
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страницы 133-141
Triphenylantimony(V) Catecholates Based on o-Quinones, Derivatives of Benzo[b][1,4]-Dioxines and Benzo[b][1,4]-Dioxepines
Тип публикации: Journal Article
Дата публикации: 2019-02-01
scimago Q4
wos Q4
БС2
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Краткое описание
New catecholate complexes of triphenylantimony(V), (Etgly-3,6-DBCat)SbPh3 (I), (Propgly-3,6-DBCat)SbPh3 (II), and (Cat-3,6-DBCat)SbPh3 (III), based on analogs of sterically hindered 3,6-di-tert-butyl-o-benzoquinone, 5,8-di-tert-butyl-2,3-dihydrobenzo[b][1,4]dioxine-6,7-dione (L1), 6,9-di-tert-butyl-2,3-dihydrobenzo[b][1,4]dioxepine-7,8-dione (L2), and 1,4-di-tert-butyl-dibenzo[b,e][1,4]dioxine-2,3-dione (L3), which are the 2,3-dihydrobenzo[b][1,4]dioxine, 2,3-dihydrobenzo[b][1,4]dioxepine, and dibenzo[1,4]dioxine derivatives, respectively, have been synthesized. At room temperature catecholates I and II react with molecular oxygen adding an O2 molecule to form the corresponding spiroendoperoxides IV and V. Catecholate III reacts with oxygen with the deep oxidation of the complex and formation of neutral o-benzoquinone. The molecular structures of complexes I and III are determined by X-ray diffraction analysis (CIF files CCDC nos. 1840299 (I · toluene) and 1840300 (III)).
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Poddelskii A. I. et al. Triphenylantimony(V) Catecholates Based on o-Quinones, Derivatives of Benzo[b][1,4]-Dioxines and Benzo[b][1,4]-Dioxepines // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2019. Vol. 45. No. 2. pp. 133-141.
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Poddelskii A. I., Okhlopkova L. S., Meshcheryakova I. N., Druzhkov N. O., Smolyaninov I. V., Fukin G. K. Triphenylantimony(V) Catecholates Based on o-Quinones, Derivatives of Benzo[b][1,4]-Dioxines and Benzo[b][1,4]-Dioxepines // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2019. Vol. 45. No. 2. pp. 133-141.
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TY - JOUR
DO - 10.1134/S1070328419010093
UR - https://doi.org/10.1134/S1070328419010093
TI - Triphenylantimony(V) Catecholates Based on o-Quinones, Derivatives of Benzo[b][1,4]-Dioxines and Benzo[b][1,4]-Dioxepines
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Poddelskii, A I
AU - Okhlopkova, L S
AU - Meshcheryakova, I N
AU - Druzhkov, N. O.
AU - Smolyaninov, I V
AU - Fukin, G. K.
PY - 2019
DA - 2019/02/01
PB - Pleiades Publishing
SP - 133-141
IS - 2
VL - 45
SN - 1070-3284
SN - 1608-3318
ER -
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@article{2019_Poddelskii,
author = {A I Poddelskii and L S Okhlopkova and I N Meshcheryakova and N. O. Druzhkov and I V Smolyaninov and G. K. Fukin},
title = {Triphenylantimony(V) Catecholates Based on o-Quinones, Derivatives of Benzo[b][1,4]-Dioxines and Benzo[b][1,4]-Dioxepines},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2019},
volume = {45},
publisher = {Pleiades Publishing},
month = {feb},
url = {https://doi.org/10.1134/S1070328419010093},
number = {2},
pages = {133--141},
doi = {10.1134/S1070328419010093}
}
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Poddelskii, A. I., et al. “Triphenylantimony(V) Catecholates Based on o-Quinones, Derivatives of Benzo[b][1,4]-Dioxines and Benzo[b][1,4]-Dioxepines.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 45, no. 2, Feb. 2019, pp. 133-141. https://doi.org/10.1134/S1070328419010093.