SNHAr Reaction of Pyridines with Bis(polyfluoroalkyl)phosphonates Assisted by Electron-Deficient Acetylenes
Publication type: Journal Article
Publication date: 2022-09-01
scimago Q4
wos Q4
SJR: 0.179
CiteScore: 1.4
Impact factor: 0.8
ISSN: 10703632, 16083350
General Chemistry
Abstract
The SNHAr reaction of pyridines with bis(polyfluoroalkyl)phosphonates assisted by benzoylphenylacetylene (equimolar reactants ratio, 70–75°С, 3.5–7 h, catalyst- and solvent-free) has led to bis(polyfluoroalkyl)pyridinylphosphonates in yield up to 51%. In the presence of phenylcyanoacetylene, pyridine has reacted with bis(2,2,2-trifluoroethyl)phosphonate at room temperature to regio- and stereoselectively form Z-(cyanophenylethenyl)-1,4-dihydropyridin-4-ylphosphonate, the SNHAr reaction kinetic product, in high yield.
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Volkov P. A. et al. SNHAr Reaction of Pyridines with Bis(polyfluoroalkyl)phosphonates Assisted by Electron-Deficient Acetylenes // Russian Journal of General Chemistry. 2022. Vol. 92. No. 9. pp. 1712-1719.
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Volkov P. A., Khrapova K. O., Telezhkin A. A., Albanov A. I., Apatrsin K. A., Trofimov B. A. SNHAr Reaction of Pyridines with Bis(polyfluoroalkyl)phosphonates Assisted by Electron-Deficient Acetylenes // Russian Journal of General Chemistry. 2022. Vol. 92. No. 9. pp. 1712-1719.
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TY - JOUR
DO - 10.1134/s1070363222090134
UR - https://link.springer.com/10.1134/S1070363222090134
TI - SNHAr Reaction of Pyridines with Bis(polyfluoroalkyl)phosphonates Assisted by Electron-Deficient Acetylenes
T2 - Russian Journal of General Chemistry
AU - Volkov, P A
AU - Khrapova, K O
AU - Telezhkin, Anton A
AU - Albanov, A I
AU - Apatrsin, K. A.
AU - Trofimov, B. A.
PY - 2022
DA - 2022/09/01
PB - Pleiades Publishing
SP - 1712-1719
IS - 9
VL - 92
SN - 1070-3632
SN - 1608-3350
ER -
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@article{2022_Volkov,
author = {P A Volkov and K O Khrapova and Anton A Telezhkin and A I Albanov and K. A. Apatrsin and B. A. Trofimov},
title = {SNHAr Reaction of Pyridines with Bis(polyfluoroalkyl)phosphonates Assisted by Electron-Deficient Acetylenes},
journal = {Russian Journal of General Chemistry},
year = {2022},
volume = {92},
publisher = {Pleiades Publishing},
month = {sep},
url = {https://link.springer.com/10.1134/S1070363222090134},
number = {9},
pages = {1712--1719},
doi = {10.1134/s1070363222090134}
}
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Volkov, P. A., et al. “SNHAr Reaction of Pyridines with Bis(polyfluoroalkyl)phosphonates Assisted by Electron-Deficient Acetylenes.” Russian Journal of General Chemistry, vol. 92, no. 9, Sep. 2022, pp. 1712-1719. https://link.springer.com/10.1134/S1070363222090134.
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