Cross-coupling of 4,5,6,7-tetrahydroindole with functionalized haloacetylenes on active surfaces of metal oxides and salts
L N Sobenina
1
,
D N Tomilin
1
,
O V Petrova
1
,
N Gulia
2
,
K Osowska
2
,
S Szafert
3
,
A.I. Mikhaleva
1
,
B. A. Trofimov
1
3
Wroclaw Research Center EIT+ Ltd., Wroclaw, Poland
|
Тип публикации: Journal Article
Дата публикации: 2010-09-01
scimago Q4
wos Q4
БС3
SJR: 0.190
CiteScore: 1.3
Impact factor: 0.9
ISSN: 10704280, 16083393
Organic Chemistry
Краткое описание
Screening was performed of metal oxides (MgO, CaO, ZnO, BaO, Al2O3, TiO2, ZrO2) and salts (CaCO3, K2CO3, ZrSiO4) as active surfaces for the reaction of ethynylation of 4,5,6,7-tetrahydroindole with ethyl bromopropynoate and bromobenzoylacetylene. It was established that Ca, Mg, Zn, and Ba oxides assist the ethynylation of 4,5,6,7-tetrahydroindole, and their activity in the reaction with ethyl bromopropynoate considerably exceeds that of aluminum oxide. The ethynylation is accompanied with the formation of intermediate E-2-(1-bromoethenyl)-4,5,6,7-tetrahydroindole and side 1,1-di(4,5,6,7-tetrahydroindol-2-yl)ethenes and 1,1-di(4,5,6,7-tetrahydroindol-2-yl)bromoethanes.
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ГОСТ
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Sobenina L. N. et al. Cross-coupling of 4,5,6,7-tetrahydroindole with functionalized haloacetylenes on active surfaces of metal oxides and salts // Russian Journal of Organic Chemistry. 2010. Vol. 46. No. 9. pp. 1373-1377.
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Sobenina L. N., Tomilin D. N., Petrova O. V., Gulia N., Osowska K., Szafert S., Mikhaleva A., Trofimov B. A. Cross-coupling of 4,5,6,7-tetrahydroindole with functionalized haloacetylenes on active surfaces of metal oxides and salts // Russian Journal of Organic Chemistry. 2010. Vol. 46. No. 9. pp. 1373-1377.
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TY - JOUR
DO - 10.1134/s1070428010090186
UR - https://doi.org/10.1134/s1070428010090186
TI - Cross-coupling of 4,5,6,7-tetrahydroindole with functionalized haloacetylenes on active surfaces of metal oxides and salts
T2 - Russian Journal of Organic Chemistry
AU - Sobenina, L N
AU - Tomilin, D N
AU - Petrova, O V
AU - Gulia, N
AU - Osowska, K
AU - Szafert, S
AU - Mikhaleva, A.I.
AU - Trofimov, B. A.
PY - 2010
DA - 2010/09/01
PB - Pleiades Publishing
SP - 1373-1377
IS - 9
VL - 46
SN - 1070-4280
SN - 1608-3393
ER -
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BibTex (до 50 авторов)
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@article{2010_Sobenina,
author = {L N Sobenina and D N Tomilin and O V Petrova and N Gulia and K Osowska and S Szafert and A.I. Mikhaleva and B. A. Trofimov},
title = {Cross-coupling of 4,5,6,7-tetrahydroindole with functionalized haloacetylenes on active surfaces of metal oxides and salts},
journal = {Russian Journal of Organic Chemistry},
year = {2010},
volume = {46},
publisher = {Pleiades Publishing},
month = {sep},
url = {https://doi.org/10.1134/s1070428010090186},
number = {9},
pages = {1373--1377},
doi = {10.1134/s1070428010090186}
}
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MLA
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Sobenina, L. N., et al. “Cross-coupling of 4,5,6,7-tetrahydroindole with functionalized haloacetylenes on active surfaces of metal oxides and salts.” Russian Journal of Organic Chemistry, vol. 46, no. 9, Sep. 2010, pp. 1373-1377. https://doi.org/10.1134/s1070428010090186.