2-chloro-3,3,5-trimethyl-2,3-dihydro-1,2λ5-oxaphosphole 2-oxide as precursor in a new synthesis of dialkyl(diaryl)-(2-methyl-4-oxopent- 2-yl)phosphine oxides
D A Tatarinov
1
,
A A Kostin
1
,
T A Baronova
1
,
A B Dobrynin
1
,
E V Mironova
1
,
D.B. Krivolapov
1
,
B I Buzykin
1
,
Publication type: Journal Article
Publication date: 2013-04-01
scimago Q4
wos Q4
SJR: 0.190
CiteScore: 1.3
Impact factor: 0.9
ISSN: 10704280, 16083393
Organic Chemistry
Abstract
A new approach has been developed to the synthesis of dialkyl(diaryl)(2-methyl-4-oxopent-2-yl)-phosphine oxides that are structural analogs of the drug dimephosphon. This approach is based on the reaction of 2-chloro-3,3,5-trimethyl-3H-1,2λ5-oxaphosphole 2-oxide with Grignard compounds, and it ensures high yields of the target products. The structure of bis(2-methoxyphenyl)(2-methyl-4-oxopent-2-yl)phosphine oxide was determined by X-ray analysis. (2-Methyl-4-oxopent-2-yl)dipropylphosphine oxide with magnesium bromide formed a 4: 1 complex whose structure was also determined by X-ray analysis.
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Tatarinov D. A. et al. 2-chloro-3,3,5-trimethyl-2,3-dihydro-1,2λ5-oxaphosphole 2-oxide as precursor in a new synthesis of dialkyl(diaryl)-(2-methyl-4-oxopent- 2-yl)phosphine oxides // Russian Journal of Organic Chemistry. 2013. Vol. 49. No. 4. pp. 516-525.
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Tatarinov D. A., Kostin A. A., Baronova T. A., Dobrynin A. B., Mironova E. V., Krivolapov D., Buzykin B. I., Mironov V. F. 2-chloro-3,3,5-trimethyl-2,3-dihydro-1,2λ5-oxaphosphole 2-oxide as precursor in a new synthesis of dialkyl(diaryl)-(2-methyl-4-oxopent- 2-yl)phosphine oxides // Russian Journal of Organic Chemistry. 2013. Vol. 49. No. 4. pp. 516-525.
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TY - JOUR
DO - 10.1134/S1070428013040040
UR - https://doi.org/10.1134/S1070428013040040
TI - 2-chloro-3,3,5-trimethyl-2,3-dihydro-1,2λ5-oxaphosphole 2-oxide as precursor in a new synthesis of dialkyl(diaryl)-(2-methyl-4-oxopent- 2-yl)phosphine oxides
T2 - Russian Journal of Organic Chemistry
AU - Tatarinov, D A
AU - Kostin, A A
AU - Baronova, T A
AU - Dobrynin, A B
AU - Mironova, E V
AU - Krivolapov, D.B.
AU - Buzykin, B I
AU - Mironov, V F
PY - 2013
DA - 2013/04/01
PB - Pleiades Publishing
SP - 516-525
IS - 4
VL - 49
SN - 1070-4280
SN - 1608-3393
ER -
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BibTex (up to 50 authors)
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@article{2013_Tatarinov,
author = {D A Tatarinov and A A Kostin and T A Baronova and A B Dobrynin and E V Mironova and D.B. Krivolapov and B I Buzykin and V F Mironov},
title = {2-chloro-3,3,5-trimethyl-2,3-dihydro-1,2λ5-oxaphosphole 2-oxide as precursor in a new synthesis of dialkyl(diaryl)-(2-methyl-4-oxopent- 2-yl)phosphine oxides},
journal = {Russian Journal of Organic Chemistry},
year = {2013},
volume = {49},
publisher = {Pleiades Publishing},
month = {apr},
url = {https://doi.org/10.1134/S1070428013040040},
number = {4},
pages = {516--525},
doi = {10.1134/S1070428013040040}
}
Cite this
MLA
Copy
Tatarinov, D. A., et al. “2-chloro-3,3,5-trimethyl-2,3-dihydro-1,2λ5-oxaphosphole 2-oxide as precursor in a new synthesis of dialkyl(diaryl)-(2-methyl-4-oxopent- 2-yl)phosphine oxides.” Russian Journal of Organic Chemistry, vol. 49, no. 4, Apr. 2013, pp. 516-525. https://doi.org/10.1134/S1070428013040040.