Aminomethylation of 2,4-Dioxo-3-azaspiro[5.5]undecane- 1,5-dicarbonitrile. Efficient Synthesis of New 3,7-Diazaspiro- [bicyclo[3.3.1]nonane-9,1′-cyclohexane] Derivatives
A N Khrustaleva
1, 2
,
K A Frolov
1, 3
,
V V Dotsenko
4, 5
,
N A Aksenov
5
,
I V Aksenova
5
,
B S Krivokolysko
3
,
S G Krivokolysko
1, 3
1
Vladimir Dal’ Lugansk National University, Lugansk, Ukraine
|
2
Taras Shevchenko Lugansk National University, Lugansk, Ukraine
|
Publication type: Journal Article
Publication date: 2018-12-01
scimago Q4
wos Q4
SJR: 0.190
CiteScore: 1.3
Impact factor: 0.9
ISSN: 10704280, 16083393
Organic Chemistry
Abstract
2,4-Dioxo-3-azaspiro[5.5]undecane-1,5-dicarbonitrile reacted with primary amines and formaldehyde on heating in boiling ethanol to give mixtures of 7-alkyl-2,4-dioxo-3,7-diazaspiro[bicyclo[3.3.1]nonane- 9,1′-cyclohexane]-1,5-dicarbonitriles and their ammonium salts. The former were isolated in 26–71% after acidification of the reaction mixture.
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Khrustaleva A. N. et al. Aminomethylation of 2,4-Dioxo-3-azaspiro[5.5]undecane- 1,5-dicarbonitrile. Efficient Synthesis of New 3,7-Diazaspiro- [bicyclo[3.3.1]nonane-9,1′-cyclohexane] Derivatives // Russian Journal of Organic Chemistry. 2018. Vol. 54. No. 12. pp. 1803-1806.
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Khrustaleva A. N., Frolov K. A., Dotsenko V. V., Aksenov N. A., Aksenova I. V., Krivokolysko B. S., Krivokolysko S. G. Aminomethylation of 2,4-Dioxo-3-azaspiro[5.5]undecane- 1,5-dicarbonitrile. Efficient Synthesis of New 3,7-Diazaspiro- [bicyclo[3.3.1]nonane-9,1′-cyclohexane] Derivatives // Russian Journal of Organic Chemistry. 2018. Vol. 54. No. 12. pp. 1803-1806.
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TY - JOUR
DO - 10.1134/s1070428018120114
UR - https://doi.org/10.1134/s1070428018120114
TI - Aminomethylation of 2,4-Dioxo-3-azaspiro[5.5]undecane- 1,5-dicarbonitrile. Efficient Synthesis of New 3,7-Diazaspiro- [bicyclo[3.3.1]nonane-9,1′-cyclohexane] Derivatives
T2 - Russian Journal of Organic Chemistry
AU - Khrustaleva, A N
AU - Frolov, K A
AU - Dotsenko, V V
AU - Aksenov, N A
AU - Aksenova, I V
AU - Krivokolysko, B S
AU - Krivokolysko, S G
PY - 2018
DA - 2018/12/01
PB - Pleiades Publishing
SP - 1803-1806
IS - 12
VL - 54
SN - 1070-4280
SN - 1608-3393
ER -
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@article{2018_Khrustaleva,
author = {A N Khrustaleva and K A Frolov and V V Dotsenko and N A Aksenov and I V Aksenova and B S Krivokolysko and S G Krivokolysko},
title = {Aminomethylation of 2,4-Dioxo-3-azaspiro[5.5]undecane- 1,5-dicarbonitrile. Efficient Synthesis of New 3,7-Diazaspiro- [bicyclo[3.3.1]nonane-9,1′-cyclohexane] Derivatives},
journal = {Russian Journal of Organic Chemistry},
year = {2018},
volume = {54},
publisher = {Pleiades Publishing},
month = {dec},
url = {https://doi.org/10.1134/s1070428018120114},
number = {12},
pages = {1803--1806},
doi = {10.1134/s1070428018120114}
}
Cite this
MLA
Copy
Khrustaleva, A. N., et al. “Aminomethylation of 2,4-Dioxo-3-azaspiro[5.5]undecane- 1,5-dicarbonitrile. Efficient Synthesis of New 3,7-Diazaspiro- [bicyclo[3.3.1]nonane-9,1′-cyclohexane] Derivatives.” Russian Journal of Organic Chemistry, vol. 54, no. 12, Dec. 2018, pp. 1803-1806. https://doi.org/10.1134/s1070428018120114.