Peculiar Features of the Reduction of Keto Group in the Synthesis of Mono- and Dialkyl-Substituted Benzo[b]benzo[4,5]thieno[2,3-d]thiophene
I. O. Gudkova
1
,
E. A. Sorokina
1
,
E A Zaborin
1
,
M S Polinskaya
1
,
O V Borshchev
1
,
S A Ponomarenko
1, 2
Publication type: Journal Article
Publication date: 2024-06-01
scimago Q4
wos Q4
SJR: 0.190
CiteScore: 1.3
Impact factor: 0.9
ISSN: 10704280, 16083393
Abstract
Mono- and dioctyl-substituted benzo[b]benzo[4,5]thieno[2,3-d]thiophenes C8-BTBT and C8-BTBT-C8 that are widely used as organic semiconductors in the manufacture of various organic electronic devices have been synthesized in two steps, by Friedel–Crafts acylation of benzo[b]benzo[4,5]thieno[2,3-d]thiophene (BTBT) and subsequent reduction of the ketone group(s). Taking into account that the limiting stage in the synthesis of such compounds is the reduction stage, different methods for the reduction acyl-substituted BTBT derivatives have been studied and probable reduction mechanisms have been proposed. The best results in the keto group reduction stage have been obtained with the use of hydrazine hydrate as reducing agent.
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7
Total citations:
7
Citations from 2024:
7
(100%)
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Gudkova I. O. et al. Peculiar Features of the Reduction of Keto Group in the Synthesis of Mono- and Dialkyl-Substituted Benzo[b]benzo[4,5]thieno[2,3-d]thiophene // Russian Journal of Organic Chemistry. 2024. Vol. 60. No. 6. pp. 1074-1085.
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Gudkova I. O., Sorokina E. A., Zaborin E. A., Polinskaya M. S., Borshchev O. V., Ponomarenko S. A. Peculiar Features of the Reduction of Keto Group in the Synthesis of Mono- and Dialkyl-Substituted Benzo[b]benzo[4,5]thieno[2,3-d]thiophene // Russian Journal of Organic Chemistry. 2024. Vol. 60. No. 6. pp. 1074-1085.
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TY - JOUR
DO - 10.1134/s1070428024060137
UR - https://link.springer.com/10.1134/S1070428024060137
TI - Peculiar Features of the Reduction of Keto Group in the Synthesis of Mono- and Dialkyl-Substituted Benzo[b]benzo[4,5]thieno[2,3-d]thiophene
T2 - Russian Journal of Organic Chemistry
AU - Gudkova, I. O.
AU - Sorokina, E. A.
AU - Zaborin, E A
AU - Polinskaya, M S
AU - Borshchev, O V
AU - Ponomarenko, S A
PY - 2024
DA - 2024/06/01
PB - Pleiades Publishing
SP - 1074-1085
IS - 6
VL - 60
SN - 1070-4280
SN - 1608-3393
ER -
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BibTex (up to 50 authors)
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@article{2024_Gudkova,
author = {I. O. Gudkova and E. A. Sorokina and E A Zaborin and M S Polinskaya and O V Borshchev and S A Ponomarenko},
title = {Peculiar Features of the Reduction of Keto Group in the Synthesis of Mono- and Dialkyl-Substituted Benzo[b]benzo[4,5]thieno[2,3-d]thiophene},
journal = {Russian Journal of Organic Chemistry},
year = {2024},
volume = {60},
publisher = {Pleiades Publishing},
month = {jun},
url = {https://link.springer.com/10.1134/S1070428024060137},
number = {6},
pages = {1074--1085},
doi = {10.1134/s1070428024060137}
}
Cite this
MLA
Copy
Gudkova, I. O., et al. “Peculiar Features of the Reduction of Keto Group in the Synthesis of Mono- and Dialkyl-Substituted Benzo[b]benzo[4,5]thieno[2,3-d]thiophene.” Russian Journal of Organic Chemistry, vol. 60, no. 6, Jun. 2024, pp. 1074-1085. https://link.springer.com/10.1134/S1070428024060137.
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