Dispersion copolymerization of methyl methacrylate and styrene in supercritical carbon dioxide
Тип публикации: Journal Article
Дата публикации: 2010-12-01
scimago Q4
БС2
SJR: 0.244
CiteScore: 2.6
Impact factor: —
ISSN: 19907931, 19907923
Physical and Theoretical Chemistry
Краткое описание
A method for producing finely dispersed powders of methyl methacrylate (MMA)-styrene copolymer by radical polymerization in a supercritical carbon dioxide medium (SC-CO2) was proposed, studied, and experimentally implemented. The dispersing agent (surfactant), which made it possible to obtain nearly monodisperse size distribution of polymer particles, was poly(dimethylsiloxane methacrylate), a SC-CO2-soluble substance. The copolymer, synthesized with a molecular mass of Mw ∼ 36000 in the form of spherical particles with a characteristic size of ∼1 μm, exhibited a higher thermal stability as compared to poly(methyl methacrylate) with a similar molecular mass. Varying the percentage ratio between MMA and styrene monomers, it was possible effectively control the integral hydrophobicity and physicomechanical characteristics of the methacrylate-styrene copolymer.
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Russian Journal of Physical Chemistry B
2 публикации, 40%
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Journal of Supercritical Fluids
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Polymer International
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Elsevier
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Pleiades Publishing
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Timashev P. S. et al. Dispersion copolymerization of methyl methacrylate and styrene in supercritical carbon dioxide // Russian Journal of Physical Chemistry B. 2010. Vol. 4. No. 7. pp. 1158-1163.
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Timashev P. S., Krotova L. I., Lemenovskii D. A., Popov V. Dispersion copolymerization of methyl methacrylate and styrene in supercritical carbon dioxide // Russian Journal of Physical Chemistry B. 2010. Vol. 4. No. 7. pp. 1158-1163.
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TY - JOUR
DO - 10.1134/S199079311007016X
UR - http://link.springer.com/10.1134/S199079311007016X
TI - Dispersion copolymerization of methyl methacrylate and styrene in supercritical carbon dioxide
T2 - Russian Journal of Physical Chemistry B
AU - Timashev, P S
AU - Krotova, L I
AU - Lemenovskii, D A
AU - Popov, V.K.
PY - 2010
DA - 2010/12/01
PB - Pleiades Publishing
SP - 1158-1163
IS - 7
VL - 4
SN - 1990-7931
SN - 1990-7923
ER -
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@article{2010_Timashev,
author = {P S Timashev and L I Krotova and D A Lemenovskii and V.K. Popov},
title = {Dispersion copolymerization of methyl methacrylate and styrene in supercritical carbon dioxide},
journal = {Russian Journal of Physical Chemistry B},
year = {2010},
volume = {4},
publisher = {Pleiades Publishing},
month = {dec},
url = {http://link.springer.com/10.1134/S199079311007016X},
number = {7},
pages = {1158--1163},
doi = {10.1134/S199079311007016X}
}
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Timashev, P. S., et al. “Dispersion copolymerization of methyl methacrylate and styrene in supercritical carbon dioxide.” Russian Journal of Physical Chemistry B, vol. 4, no. 7, Dec. 2010, pp. 1158-1163. http://link.springer.com/10.1134/S199079311007016X.