Inorganic Materials: Applied Research, volume 11, issue 2, pages 385-393
Optimization of Conditions for Synthesis of Ultrafine Silver Particles in Hemp Fiber Extract
Publication type: Journal Article
Publication date: 2020-03-01
Quartile SCImago
Q3
Quartile WOS
—
Impact factor: —
ISSN: 20751133, 2075115X
General Materials Science
General Engineering
Abstract
The impact of conditions in extraction of natural admixtures (pectin compounds, hemicelluloses, and lignin) from hemp fiber during chemical modification of fibrous mass was studied. It was shown that the maximum extraction of admixtures requires increasing the temperature of fiber treatment to 100°С and the sodium hydroxide concentration to 10 g/L. Using infrared spectroscopy and potentiometric titration methods, it was proved that the increase in alkalinity of the boiling liquor leads not only to the increase in the amount of admixtures in the liquor but also to their destruction, while the complex of reducing ingredients that was formed in the liquor can act as a reductant of silver ions even under conditions of low temperatures in extraction. The kinetics of reduction of silver ions in the extract liquor was investigated. The correlation of the efficiency of the reduction of silver ions and the quantitative content of admixtures in the liquor was found. Using photon correlation spectroscopy, it was shown that reduction in an extract obtained under high alkalinity makes it possible to obtain particles of small size, not more than 30 nm. It was proved that the antimicrobial activity of synthesized sols and cellulosic materials treated with these sols against test cultures depends on the synthesis conditions.
Top-30
Citations by journals
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E3S Web of Conferences
1 publication, 25%
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Coloration Technology
1 publication, 25%
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Journal of Natural Fibers
1 publication, 25%
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Russian Chemical Reviews
1 publication, 25%
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Citations by publishers
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1
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EDP Sciences
1 publication, 25%
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Wiley
1 publication, 25%
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Taylor & Francis
1 publication, 25%
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Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii
1 publication, 25%
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1
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Dymnikova N. S. et al. Optimization of Conditions for Synthesis of Ultrafine Silver Particles in Hemp Fiber Extract // Inorganic Materials: Applied Research. 2020. Vol. 11. No. 2. pp. 385-393.
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Dymnikova N. S., Erohina E. V., Moryganov A. P., Grigorev S. V., Kuznetsov O. Yu. Optimization of Conditions for Synthesis of Ultrafine Silver Particles in Hemp Fiber Extract // Inorganic Materials: Applied Research. 2020. Vol. 11. No. 2. pp. 385-393.
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TY - JOUR
DO - 10.1134/s2075113320020082
UR - https://doi.org/10.1134/s2075113320020082
TI - Optimization of Conditions for Synthesis of Ultrafine Silver Particles in Hemp Fiber Extract
T2 - Inorganic Materials: Applied Research
AU - Dymnikova, N S
AU - Erohina, E V
AU - Moryganov, A P
AU - Grigorev, S V
AU - Kuznetsov, O Yu
PY - 2020
DA - 2020/03/01 00:00:00
PB - Pleiades Publishing
SP - 385-393
IS - 2
VL - 11
SN - 2075-1133
SN - 2075-115X
ER -
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@article{2020_Dymnikova,
author = {N S Dymnikova and E V Erohina and A P Moryganov and S V Grigorev and O Yu Kuznetsov},
title = {Optimization of Conditions for Synthesis of Ultrafine Silver Particles in Hemp Fiber Extract},
journal = {Inorganic Materials: Applied Research},
year = {2020},
volume = {11},
publisher = {Pleiades Publishing},
month = {mar},
url = {https://doi.org/10.1134/s2075113320020082},
number = {2},
pages = {385--393},
doi = {10.1134/s2075113320020082}
}
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Dymnikova, N. S., et al. “Optimization of Conditions for Synthesis of Ultrafine Silver Particles in Hemp Fiber Extract.” Inorganic Materials: Applied Research, vol. 11, no. 2, Mar. 2020, pp. 385-393. https://doi.org/10.1134/s2075113320020082.