Preparation of High-Purity Tin Dichloride
Publication type: Journal Article
Publication date: 2022-02-01
scimago Q4
wos Q4
SJR: 0.183
CiteScore: 1.3
Impact factor: 0.7
ISSN: 00201685, 16083172
Materials Chemistry
Metals and Alloys
Inorganic Chemistry
General Chemical Engineering
Abstract
Extrapure-grade (99.9985 wt % pure) SnCl2 has been prepared from commercially pure metallic tin and hydrogen chloride gas. Purifying the synthesized tin(II) chloride in a fractional distillation column under normal conditions, we obtained extrapure-grade SnCl2 containing under 1 ppm impurities. The samples thus prepared were characterized by inductively coupled plasma mass spectrometry, IR and Raman spectroscopies, and X-ray diffraction.
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Mastryukov M. V. et al. Preparation of High-Purity Tin Dichloride // Inorganic Materials. 2022. Vol. 58. No. 2. pp. 177-182.
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Mastryukov M. V., Brekhovskikh M. N., Demina L. I., Moiseeva L., Fedorov V. Preparation of High-Purity Tin Dichloride // Inorganic Materials. 2022. Vol. 58. No. 2. pp. 177-182.
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TY - JOUR
DO - 10.1134/s0020168522020108
UR - https://doi.org/10.1134/s0020168522020108
TI - Preparation of High-Purity Tin Dichloride
T2 - Inorganic Materials
AU - Mastryukov, M V
AU - Brekhovskikh, M N
AU - Demina, L. I.
AU - Moiseeva, L.V.
AU - Fedorov, V.A.
PY - 2022
DA - 2022/02/01
PB - Pleiades Publishing
SP - 177-182
IS - 2
VL - 58
SN - 0020-1685
SN - 1608-3172
ER -
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BibTex (up to 50 authors)
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@article{2022_Mastryukov,
author = {M V Mastryukov and M N Brekhovskikh and L. I. Demina and L.V. Moiseeva and V.A. Fedorov},
title = {Preparation of High-Purity Tin Dichloride},
journal = {Inorganic Materials},
year = {2022},
volume = {58},
publisher = {Pleiades Publishing},
month = {feb},
url = {https://doi.org/10.1134/s0020168522020108},
number = {2},
pages = {177--182},
doi = {10.1134/s0020168522020108}
}
Cite this
MLA
Copy
Mastryukov, M. V., et al. “Preparation of High-Purity Tin Dichloride.” Inorganic Materials, vol. 58, no. 2, Feb. 2022, pp. 177-182. https://doi.org/10.1134/s0020168522020108.