volume 58 issue 4 pages 349-355

Synthesis and Phase Transformations of Compounds in the Mg4Na(PO4)3–Mg3(PO4)2 System as Promising Phases for the Fabrication of Bioceramics

Publication typeJournal Article
Publication date2022-04-01
scimago Q4
wos Q4
SJR0.183
CiteScore1.3
Impact factor0.7
ISSN00201685, 16083172
Materials Chemistry
Metals and Alloys
Inorganic Chemistry
General Chemical Engineering
Abstract
Phase transformations of the magnesium sodium double phosphates Mg4Na(PO4)3 and MgNaPO4 in the Mg4Na(PO4)3–Mg3(PO4)2 system have been studied by thermal analysis and X-ray diffraction. Optimal conditions for the preparation of phase-pure MgNaPO4 are ensured by solid-state synthesis with heat treatment at 900°C, followed by additional firing at 600°C, which is related to the polymorphic transformations of this phase at temperatures of 893 and 727°C. The polymorphism of Mg4Na(PO4)3 has been studied in detail. It has been shown that this compound undergo a polymorphic transformation at 1025°C and decompose incongruently at 1141°C. The synthesized compounds can be used as a basis for the fabrication of bioceramic materials for osteoplasty.
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Preobrazhenskiy I. I., Putlyaev V. I. Synthesis and Phase Transformations of Compounds in the Mg4Na(PO4)3–Mg3(PO4)2 System as Promising Phases for the Fabrication of Bioceramics // Inorganic Materials. 2022. Vol. 58. No. 4. pp. 349-355.
GOST all authors (up to 50) Copy
Preobrazhenskiy I. I., Putlyaev V. I. Synthesis and Phase Transformations of Compounds in the Mg4Na(PO4)3–Mg3(PO4)2 System as Promising Phases for the Fabrication of Bioceramics // Inorganic Materials. 2022. Vol. 58. No. 4. pp. 349-355.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1134/s0020168522030128
UR - https://doi.org/10.1134/s0020168522030128
TI - Synthesis and Phase Transformations of Compounds in the Mg4Na(PO4)3–Mg3(PO4)2 System as Promising Phases for the Fabrication of Bioceramics
T2 - Inorganic Materials
AU - Preobrazhenskiy, I I
AU - Putlyaev, V I
PY - 2022
DA - 2022/04/01
PB - Pleiades Publishing
SP - 349-355
IS - 4
VL - 58
SN - 0020-1685
SN - 1608-3172
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2022_Preobrazhenskiy,
author = {I I Preobrazhenskiy and V I Putlyaev},
title = {Synthesis and Phase Transformations of Compounds in the Mg4Na(PO4)3–Mg3(PO4)2 System as Promising Phases for the Fabrication of Bioceramics},
journal = {Inorganic Materials},
year = {2022},
volume = {58},
publisher = {Pleiades Publishing},
month = {apr},
url = {https://doi.org/10.1134/s0020168522030128},
number = {4},
pages = {349--355},
doi = {10.1134/s0020168522030128}
}
MLA
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Preobrazhenskiy, I. I., and V I Putlyaev. “Synthesis and Phase Transformations of Compounds in the Mg4Na(PO4)3–Mg3(PO4)2 System as Promising Phases for the Fabrication of Bioceramics.” Inorganic Materials, vol. 58, no. 4, Apr. 2022, pp. 349-355. https://doi.org/10.1134/s0020168522030128.