CRYSTAL STRUCTURE OF ZINC LACTATE DIHYDRATE – A BY-PRODUCT OF THE MICELLAR SYNTHESIS OF ZnO2 NANOPARTICLES FROM ZINC ACETATE AND HYDROPERITE
Publication type: Journal Article
Publication date: 2021-04-01
scimago Q4
wos Q4
SJR: 0.211
CiteScore: 1.9
Impact factor: 1.4
ISSN: 00224766, 15738779
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
The phase composition of the interaction product of zinc acetate with hydrogen peroxide in a dispersed aqueous phase of a reverse micellar solution based on oxyethylated Brij 30 surfactant and decane as a dispersion medium is analyzed by powder X-ray diffraction (XRD). Along with ZnO2 nanoparticle, the isolated product is found to contain needle-like microcrystals that, according to the single crystal XRD analysis, are zinc lactate dihydrate [Zn(lact)2(H2O)2]: a = 6.0196(3) Å, b = 11.9068(4) Å, c = 14.3878(7) Å, Z = 4, space group P212121. The coordination environment of the Zn atom is a distorted octahedron: Zn–О distances are 2.051(2)-2.099(3) Å, ∠О–Zn–О bond angles are 76.16° and 76.14°. Chelate rings are bent along the О…О line at 22.18° and 11.54°. The Hirshfeld surface (complex sphericity 0.79, asphericity 0.16) is constructed and intermolecular contacts are analyzed. A comparative crystal chemical analysis with the known [Zn(lact)2(H2O)2]·H2O structure is performed.
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Gromilov S. A., Piryazev D. A., Tatarchuk V. V. CRYSTAL STRUCTURE OF ZINC LACTATE DIHYDRATE – A BY-PRODUCT OF THE MICELLAR SYNTHESIS OF ZnO2 NANOPARTICLES FROM ZINC ACETATE AND HYDROPERITE // Journal of Structural Chemistry. 2021. Vol. 62. No. 4. pp. 571-576.
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Gromilov S. A., Piryazev D. A., Tatarchuk V. V. CRYSTAL STRUCTURE OF ZINC LACTATE DIHYDRATE – A BY-PRODUCT OF THE MICELLAR SYNTHESIS OF ZnO2 NANOPARTICLES FROM ZINC ACETATE AND HYDROPERITE // Journal of Structural Chemistry. 2021. Vol. 62. No. 4. pp. 571-576.
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TY - JOUR
DO - 10.1134/s0022476621040089
UR - https://doi.org/10.1134/s0022476621040089
TI - CRYSTAL STRUCTURE OF ZINC LACTATE DIHYDRATE – A BY-PRODUCT OF THE MICELLAR SYNTHESIS OF ZnO2 NANOPARTICLES FROM ZINC ACETATE AND HYDROPERITE
T2 - Journal of Structural Chemistry
AU - Gromilov, S. A.
AU - Piryazev, D A
AU - Tatarchuk, V V
PY - 2021
DA - 2021/04/01
PB - Pleiades Publishing
SP - 571-576
IS - 4
VL - 62
SN - 0022-4766
SN - 1573-8779
ER -
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@article{2021_Gromilov,
author = {S. A. Gromilov and D A Piryazev and V V Tatarchuk},
title = {CRYSTAL STRUCTURE OF ZINC LACTATE DIHYDRATE – A BY-PRODUCT OF THE MICELLAR SYNTHESIS OF ZnO2 NANOPARTICLES FROM ZINC ACETATE AND HYDROPERITE},
journal = {Journal of Structural Chemistry},
year = {2021},
volume = {62},
publisher = {Pleiades Publishing},
month = {apr},
url = {https://doi.org/10.1134/s0022476621040089},
number = {4},
pages = {571--576},
doi = {10.1134/s0022476621040089}
}
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Gromilov, S. A., et al. “CRYSTAL STRUCTURE OF ZINC LACTATE DIHYDRATE – A BY-PRODUCT OF THE MICELLAR SYNTHESIS OF ZnO2 NANOPARTICLES FROM ZINC ACETATE AND HYDROPERITE.” Journal of Structural Chemistry, vol. 62, no. 4, Apr. 2021, pp. 571-576. https://doi.org/10.1134/s0022476621040089.