Synthesis of sodium nickel phosphate and its crystallographic, spectroscopic, and temperature-controlled X-ray diffraction study
Publication type: Journal Article
Publication date: 2015-03-24
scimago Q3
wos Q4
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
Sodium nickel phosphate NaNiPO4 has been synthesized by crystallization from salt solutions containing corresponding metals and phosphoric acid and subsequent heat treatment. NaNiPO4 with a maricite structure has been studied by a combination of methods. Its structure has been refined by the Rietweld method (space group Pnma, a = 8.7839(2) Å, b = 6.7426(2), c = 5.0368(2) Å, V = 298.31(2) Å3, Z = 4). The structure framework is composed of edge-sharing NiO6 octahedra arranged in columns running along the b axis and linked with each other through PO4 tetrahedra. The cavities in the structure accommodate Na+ ions. No temperature-induced changes in the X-ray diffraction pattern of NaNiPO4 in the temperature range 25–700°C have been observed. The volumetric thermal expansion coefficient of the phosphate, α V = 34 × 10−6 K−1, allows one to classify it as a strongly expanding substance. Maricite structure stabilities are compared for NaEIIPO4 (EII = Mn, Fe, Co, Ni).
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Total citations:
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Citations from 2025:
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(14.29%)
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Korchemkin I. V. et al. Synthesis of sodium nickel phosphate and its crystallographic, spectroscopic, and temperature-controlled X-ray diffraction study // Russian Journal of Inorganic Chemistry. 2015. Vol. 60. No. 3. pp. 265-269.
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Korchemkin I. V., Petkov I. V., Kurazhkovskaya V. S., Borovikova E. Synthesis of sodium nickel phosphate and its crystallographic, spectroscopic, and temperature-controlled X-ray diffraction study // Russian Journal of Inorganic Chemistry. 2015. Vol. 60. No. 3. pp. 265-269.
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TY - JOUR
DO - 10.1134/s0036023615030092
UR - https://doi.org/10.1134/s0036023615030092
TI - Synthesis of sodium nickel phosphate and its crystallographic, spectroscopic, and temperature-controlled X-ray diffraction study
T2 - Russian Journal of Inorganic Chemistry
AU - Korchemkin, I V
AU - Petkov, I V
AU - Kurazhkovskaya, V S
AU - Borovikova, E.Yu.
PY - 2015
DA - 2015/03/24
PB - Pleiades Publishing
SP - 265-269
IS - 3
VL - 60
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2015_Korchemkin,
author = {I V Korchemkin and I V Petkov and V S Kurazhkovskaya and E.Yu. Borovikova},
title = {Synthesis of sodium nickel phosphate and its crystallographic, spectroscopic, and temperature-controlled X-ray diffraction study},
journal = {Russian Journal of Inorganic Chemistry},
year = {2015},
volume = {60},
publisher = {Pleiades Publishing},
month = {mar},
url = {https://doi.org/10.1134/s0036023615030092},
number = {3},
pages = {265--269},
doi = {10.1134/s0036023615030092}
}
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MLA
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Korchemkin, I. V., et al. “Synthesis of sodium nickel phosphate and its crystallographic, spectroscopic, and temperature-controlled X-ray diffraction study.” Russian Journal of Inorganic Chemistry, vol. 60, no. 3, Mar. 2015, pp. 265-269. https://doi.org/10.1134/s0036023615030092.