volume 63 issue 8 pages 993-1000

Synthesis of Calcium Phosphate and Calcium Silicate Composites

Publication typeJournal Article
Publication date2018-08-25
scimago Q3
wos Q4
SJR0.270
CiteScore3.0
Impact factor1.5
ISSN00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
A one-step method for preparing composites based on calcium phosphates (CPs) and calcium silicates (CSs) with variable contents of the components is proposed. The combination of chemical analysis, X-ray powder diffraction, and simultaneous thermal analysis with mass-spectrometric detection (STA-MS) showed that the coprecipitation of salts from aqueous solutions yielded mixtures of poorly crystallized carbonate hydroxyapatite (CHA) and xonotlite with minor calcite. Scanning electron microscopy and low-temperature nitrogen adsorption showed that nanosized crystallites of these phases during crystallization were combined into mesoporous aggregates (the mean pore size was 6–11 nm) to form micrometer-sized bulk structures with a developed surface. Two-hour calcination of synthesis products at 1000°С yielded mixtures of well-crystallized Са10(РО4)6(ОН)2 and β-CaSiO3.
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GOST |
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GOST Copy
Solonenko A. P. et al. Synthesis of Calcium Phosphate and Calcium Silicate Composites // Russian Journal of Inorganic Chemistry. 2018. Vol. 63. No. 8. pp. 993-1000.
GOST all authors (up to 50) Copy
Solonenko A. P., Blesman A. I., Polonyankin D. A., Gorbunov V. Synthesis of Calcium Phosphate and Calcium Silicate Composites // Russian Journal of Inorganic Chemistry. 2018. Vol. 63. No. 8. pp. 993-1000.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1134/s0036023618080211
UR - https://doi.org/10.1134/s0036023618080211
TI - Synthesis of Calcium Phosphate and Calcium Silicate Composites
T2 - Russian Journal of Inorganic Chemistry
AU - Solonenko, A P
AU - Blesman, A I
AU - Polonyankin, D A
AU - Gorbunov, V.A.
PY - 2018
DA - 2018/08/25
PB - Pleiades Publishing
SP - 993-1000
IS - 8
VL - 63
SN - 0036-0236
SN - 1531-8613
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2018_Solonenko,
author = {A P Solonenko and A I Blesman and D A Polonyankin and V.A. Gorbunov},
title = {Synthesis of Calcium Phosphate and Calcium Silicate Composites},
journal = {Russian Journal of Inorganic Chemistry},
year = {2018},
volume = {63},
publisher = {Pleiades Publishing},
month = {aug},
url = {https://doi.org/10.1134/s0036023618080211},
number = {8},
pages = {993--1000},
doi = {10.1134/s0036023618080211}
}
MLA
Cite this
MLA Copy
Solonenko, A. P., et al. “Synthesis of Calcium Phosphate and Calcium Silicate Composites.” Russian Journal of Inorganic Chemistry, vol. 63, no. 8, Aug. 2018, pp. 993-1000. https://doi.org/10.1134/s0036023618080211.