,
volume 46
,
issue 6
,
pages 379-385
New Gallium Hydrides with Dianionic Acenaphthene-1,2-Diimine Ligands
Publication type: Journal Article
Publication date: 2020-06-14
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
Heating of a solution of [(Dpp-bian)GaH2] (I) (Dpp-bian = 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene) in pyridine leads to elimination of a hydrogen atom and reduction of the diimine ligand to dianion, resulting in the complex [(Dpp-bian)GaH(Py)] (II). The reaction of I with 1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene (i-Pr2ImMe) is accompanied by a similar process, with the reaction product being identified as [(Dpp-bian)GaH(i-Pr2ImMe)] (III). Diamagnetic derivatives II and III were characterized by 1H NMR spectroscopy. The molecular structure of compound II was established by X-ray diffraction (CIF file CCDC no. 1973549).
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Koptseva T. S. et al. New Gallium Hydrides with Dianionic Acenaphthene-1,2-Diimine Ligands // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2020. Vol. 46. No. 6. pp. 379-385.
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Koptseva T. S., Sokolov V. G., Baranov E. V., Fedushkin I. L. New Gallium Hydrides with Dianionic Acenaphthene-1,2-Diimine Ligands // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2020. Vol. 46. No. 6. pp. 379-385.
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RIS
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TY - JOUR
DO - 10.1134/s1070328420060020
UR - https://doi.org/10.1134/s1070328420060020
TI - New Gallium Hydrides with Dianionic Acenaphthene-1,2-Diimine Ligands
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Koptseva, T S
AU - Sokolov, V. G.
AU - Baranov, E V
AU - Fedushkin, I L
PY - 2020
DA - 2020/06/14
PB - Pleiades Publishing
SP - 379-385
IS - 6
VL - 46
SN - 1070-3284
SN - 1608-3318
ER -
Cite this
BibTex (up to 50 authors)
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@article{2020_Koptseva,
author = {T S Koptseva and V. G. Sokolov and E V Baranov and I L Fedushkin},
title = {New Gallium Hydrides with Dianionic Acenaphthene-1,2-Diimine Ligands},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2020},
volume = {46},
publisher = {Pleiades Publishing},
month = {jun},
url = {https://doi.org/10.1134/s1070328420060020},
number = {6},
pages = {379--385},
doi = {10.1134/s1070328420060020}
}
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MLA
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Koptseva, T. S., et al. “New Gallium Hydrides with Dianionic Acenaphthene-1,2-Diimine Ligands.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 46, no. 6, Jun. 2020, pp. 379-385. https://doi.org/10.1134/s1070328420060020.