Reaction of 1-germatranol hydrate with carboxylic acids
2
Baria-Vung Tau University, Vung-Tau, Vietnam
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Publication type: Journal Article
Publication date: 2015-12-01
scimago Q4
wos Q4
SJR: 0.179
CiteScore: 1.4
Impact factor: 0.8
ISSN: 10703632, 16083350
General Chemistry
Abstract
Reaction of 1-germatranol hydrate with carboxylic acids RCOOH (R = ClCH2, PhCH=CH, Ph, 2-FC6H4, 3-BrC6H4, 3-HOC6H4, 3-EtOC6H4) in protic (CH3OH, iso-C5H11OH) and aprotic polar solvent (CH3CN) is studied. 1-Acyloxygermatranes RC(O)OGe(OCH{in2}CH{in2}){in3}N are formed in yields from 11 to ~100 % depending on the nature of the acid, solvent, duration of the process and the method of its completion. The reaction is the most effective in acetonitrile. Its topochemical completion (heating of the reaction residue in a vacuum) increases the yield of 1-acyloxygermatranes.
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Baryshok V. P., Le N. T. Z. Reaction of 1-germatranol hydrate with carboxylic acids // Russian Journal of General Chemistry. 2015. Vol. 85. No. 12. pp. 2748-2753.
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Baryshok V. P., Le N. T. Z. Reaction of 1-germatranol hydrate with carboxylic acids // Russian Journal of General Chemistry. 2015. Vol. 85. No. 12. pp. 2748-2753.
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RIS
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TY - JOUR
DO - 10.1134/s1070363215120154
UR - https://doi.org/10.1134/s1070363215120154
TI - Reaction of 1-germatranol hydrate with carboxylic acids
T2 - Russian Journal of General Chemistry
AU - Baryshok, V P
AU - Le, N T Z
PY - 2015
DA - 2015/12/01
PB - Pleiades Publishing
SP - 2748-2753
IS - 12
VL - 85
SN - 1070-3632
SN - 1608-3350
ER -
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BibTex (up to 50 authors)
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@article{2015_Baryshok,
author = {V P Baryshok and N T Z Le},
title = {Reaction of 1-germatranol hydrate with carboxylic acids},
journal = {Russian Journal of General Chemistry},
year = {2015},
volume = {85},
publisher = {Pleiades Publishing},
month = {dec},
url = {https://doi.org/10.1134/s1070363215120154},
number = {12},
pages = {2748--2753},
doi = {10.1134/s1070363215120154}
}
Cite this
MLA
Copy
Baryshok, V. P., and N T Z Le. “Reaction of 1-germatranol hydrate with carboxylic acids.” Russian Journal of General Chemistry, vol. 85, no. 12, Dec. 2015, pp. 2748-2753. https://doi.org/10.1134/s1070363215120154.