Catalysis of the Suzuki reaction by acyclic diaminocarbene palladium complexes generated in situ
Publication type: Journal Article
Publication date: 2016-09-01
scimago Q4
wos Q4
SJR: 0.179
CiteScore: 1.4
Impact factor: 0.8
ISSN: 10703632, 16083350
General Chemistry
Abstract
Acyclic diaminocarbene palladium complexes generated in situ by nucleophilic attack of morpholine, 4-nitrophenylhydrazine, or benzhydrazide on bis(isocyanide) palladium(II) complexes catalyzed the Suzuki reaction of 4-iodo- or 4-bromoanisole with phenylboronic acid. Morpholine turned out to be the best catalyst modifier. The cross coupling reaction under fairly mild conditions (reflux in ethanol in the presence of potassium carbonate) in 2 h afforded 4-methoxybiphenyl whose yield was insignificantly lower than in the presence of preliminarily prepared catalyst. Neither preliminary degassing nor protection from atmospheric moisture and oxygen was necessary.
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GOST
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Boyarskaya D. V., Boyarskii V. P. Catalysis of the Suzuki reaction by acyclic diaminocarbene palladium complexes generated in situ // Russian Journal of General Chemistry. 2016. Vol. 86. No. 9. pp. 2033-2036.
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Boyarskaya D. V., Boyarskii V. P. Catalysis of the Suzuki reaction by acyclic diaminocarbene palladium complexes generated in situ // Russian Journal of General Chemistry. 2016. Vol. 86. No. 9. pp. 2033-2036.
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RIS
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TY - JOUR
DO - 10.1134/s1070363216090085
UR - https://doi.org/10.1134/s1070363216090085
TI - Catalysis of the Suzuki reaction by acyclic diaminocarbene palladium complexes generated in situ
T2 - Russian Journal of General Chemistry
AU - Boyarskaya, D V
AU - Boyarskii, V P
PY - 2016
DA - 2016/09/01
PB - Pleiades Publishing
SP - 2033-2036
IS - 9
VL - 86
SN - 1070-3632
SN - 1608-3350
ER -
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BibTex (up to 50 authors)
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@article{2016_Boyarskaya,
author = {D V Boyarskaya and V P Boyarskii},
title = {Catalysis of the Suzuki reaction by acyclic diaminocarbene palladium complexes generated in situ},
journal = {Russian Journal of General Chemistry},
year = {2016},
volume = {86},
publisher = {Pleiades Publishing},
month = {sep},
url = {https://doi.org/10.1134/s1070363216090085},
number = {9},
pages = {2033--2036},
doi = {10.1134/s1070363216090085}
}
Cite this
MLA
Copy
Boyarskaya, D. V., and V P Boyarskii. “Catalysis of the Suzuki reaction by acyclic diaminocarbene palladium complexes generated in situ.” Russian Journal of General Chemistry, vol. 86, no. 9, Sep. 2016, pp. 2033-2036. https://doi.org/10.1134/s1070363216090085.
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