volume 87 issue 3 pages 442-446

New phosphorylated glycoluril derivatives

Publication typeJournal Article
Publication date2017-03-01
scimago Q4
wos Q4
SJR0.179
CiteScore1.4
Impact factor0.8
ISSN10703632, 16083350
General Chemistry
Abstract
The N-acylation of glycoluril with 1-haloacetyl halides was studied. The optimal conditions and reaction regioselectivity, as well as the effect of reagent molar ratios, base nature, temperature, and reaction time on the yield of the target product were established. It was shown that the chemical modification of the synthesized bis(bromoacetyl) derivative of glycoluril by phosphorylation by the classical Arbuzov reaction gave a previously unknown bis(diethylphosphonoacetyl) derivative of glycoluril. The consecutive silylation and hydrolysis of the latter derivative gave the corresponding bis(phosphonoacetyl) derivative which presents interest as a potentially biologically active compound.
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GOST Copy
Salkeeva L. K. et al. New phosphorylated glycoluril derivatives // Russian Journal of General Chemistry. 2017. Vol. 87. No. 3. pp. 442-446.
GOST all authors (up to 50) Copy
Salkeeva L. K., Taishibekova E. K., Bakibaev A. A., Minaeva E. V., Makin B. K., Sugralina L. M., Salkeeva A. K. New phosphorylated glycoluril derivatives // Russian Journal of General Chemistry. 2017. Vol. 87. No. 3. pp. 442-446.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1134/s1070363217030124
UR - https://doi.org/10.1134/s1070363217030124
TI - New phosphorylated glycoluril derivatives
T2 - Russian Journal of General Chemistry
AU - Salkeeva, L K
AU - Taishibekova, E K
AU - Bakibaev, A A
AU - Minaeva, E V
AU - Makin, B K
AU - Sugralina, L M
AU - Salkeeva, A K
PY - 2017
DA - 2017/03/01
PB - Pleiades Publishing
SP - 442-446
IS - 3
VL - 87
SN - 1070-3632
SN - 1608-3350
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2017_Salkeeva,
author = {L K Salkeeva and E K Taishibekova and A A Bakibaev and E V Minaeva and B K Makin and L M Sugralina and A K Salkeeva},
title = {New phosphorylated glycoluril derivatives},
journal = {Russian Journal of General Chemistry},
year = {2017},
volume = {87},
publisher = {Pleiades Publishing},
month = {mar},
url = {https://doi.org/10.1134/s1070363217030124},
number = {3},
pages = {442--446},
doi = {10.1134/s1070363217030124}
}
MLA
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MLA Copy
Salkeeva, L. K., et al. “New phosphorylated glycoluril derivatives.” Russian Journal of General Chemistry, vol. 87, no. 3, Mar. 2017, pp. 442-446. https://doi.org/10.1134/s1070363217030124.