Synthesis of C1-Symmetric Bulky Redoxi-Active Iminoketones and Diimines of the Pyrene and Aceanthrylene Series
Publication type: Journal Article
Publication date: 2023-12-01
scimago Q4
wos Q4
SJR: 0.179
CiteScore: 1.4
Impact factor: 0.8
ISSN: 10703632, 16083350
General Chemistry
Abstract
The reactions of oxialyl chloride with pyrene, 2,7-di-tert-butylpyrene, anthracene and 4,7-di-tert-butyl-1,2-dihydroacenaphthylene give the corresponding diketones: cyclopent[cd]pyrene-3,4-dione, 2,7-di-tert-butylcyclopenta[cd]pyrene-3,4-dione, aceanthrylene-1,2-dione, 1,2-diketo-3,8-di-tert-butylpyracene. The diketones react with 2,6-diisopropylaniline to form a series of the corresponding imines. It was shown that 1,2-diketo-3,8-di-tert-butylpyracene does not produce condensation products with 2,6-diisopropylaniline. The effect of the imine substituents on the electronic structure and UV spectra of the aceanthrylene derivatives was studied with by DFT and TD DFT. Structure of 1,2-diketo-3,8-di-tert-butylpyracene, as well as (E)-2-(2,6-diisopropylphenylimino)aceanthrylen-1(2H)-one and 3,4-bis[2,6-diisopropylphenylimino]aceanthrylene was characterized by single crystal X-ray diffraction.
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Lukoyanov A. N. et al. Synthesis of C1-Symmetric Bulky Redoxi-Active Iminoketones and Diimines of the Pyrene and Aceanthrylene Series // Russian Journal of General Chemistry. 2023. Vol. 93. No. S3. p. S649-S662.
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Lukoyanov A. N., Markin G. V., Zhigulin G. Y., Ketkov S. Y., Lopatin M. A., Baranov E. V., Kuropatov V. A., Belikov A. A. Synthesis of C1-Symmetric Bulky Redoxi-Active Iminoketones and Diimines of the Pyrene and Aceanthrylene Series // Russian Journal of General Chemistry. 2023. Vol. 93. No. S3. p. S649-S662.
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TY - JOUR
DO - 10.1134/s107036322316003x
UR - https://link.springer.com/10.1134/S107036322316003X
TI - Synthesis of C1-Symmetric Bulky Redoxi-Active Iminoketones and Diimines of the Pyrene and Aceanthrylene Series
T2 - Russian Journal of General Chemistry
AU - Lukoyanov, Anton N
AU - Markin, G V
AU - Zhigulin, G. Yu.
AU - Ketkov, Sergey Yu.
AU - Lopatin, M. A.
AU - Baranov, Evgeny V
AU - Kuropatov, Viacheslav A
AU - Belikov, A A
PY - 2023
DA - 2023/12/01
PB - Pleiades Publishing
SP - S649-S662
IS - S3
VL - 93
SN - 1070-3632
SN - 1608-3350
ER -
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@article{2023_Lukoyanov,
author = {Anton N Lukoyanov and G V Markin and G. Yu. Zhigulin and Sergey Yu. Ketkov and M. A. Lopatin and Evgeny V Baranov and Viacheslav A Kuropatov and A A Belikov},
title = {Synthesis of C1-Symmetric Bulky Redoxi-Active Iminoketones and Diimines of the Pyrene and Aceanthrylene Series},
journal = {Russian Journal of General Chemistry},
year = {2023},
volume = {93},
publisher = {Pleiades Publishing},
month = {dec},
url = {https://link.springer.com/10.1134/S107036322316003X},
number = {S3},
pages = {S649--S662},
doi = {10.1134/s107036322316003x}
}
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MLA
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Lukoyanov, Anton N., et al. “Synthesis of C1-Symmetric Bulky Redoxi-Active Iminoketones and Diimines of the Pyrene and Aceanthrylene Series.” Russian Journal of General Chemistry, vol. 93, no. S3, Dec. 2023, pp. S649-S662. https://link.springer.com/10.1134/S107036322316003X.