Alkyl 3-nitroacrylates: Synthesis and reactions with cyclohexane-1,3-diones and Meldrum’s acid
Publication type: Journal Article
Publication date: 2017-12-01
scimago Q4
wos Q4
SJR: 0.190
CiteScore: 1.3
Impact factor: 0.9
ISSN: 10704280, 16083393
Organic Chemistry
Abstract
A modified procedure was proposed for the synthesis of alkyl 3-nitroacrylates by nitroiodination of alkyl acrylates and subsequent dehydroiodination of iodonitropropanoates with triethylamine. Alkyl 3-nitroacrylates reacted with cyclohexane-1,3-dione, dimedone, and Meldrum’s acid in the presence of N,N,N-tri-methylanilinium hydroxide (Rodionov’s catalyst) in anhydrous methanol to give the corresponding Michael adducts.
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Pelipko V. V. et al. Alkyl 3-nitroacrylates: Synthesis and reactions with cyclohexane-1,3-diones and Meldrum’s acid // Russian Journal of Organic Chemistry. 2017. Vol. 53. No. 12. pp. 1799-1808.
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Pelipko V. V., Makarenko S. V., Baichurin R. I., Berestovitskaya V. M., Kovalenko K. S. Alkyl 3-nitroacrylates: Synthesis and reactions with cyclohexane-1,3-diones and Meldrum’s acid // Russian Journal of Organic Chemistry. 2017. Vol. 53. No. 12. pp. 1799-1808.
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TY - JOUR
DO - 10.1134/s107042801712003x
UR - https://doi.org/10.1134/s107042801712003x
TI - Alkyl 3-nitroacrylates: Synthesis and reactions with cyclohexane-1,3-diones and Meldrum’s acid
T2 - Russian Journal of Organic Chemistry
AU - Pelipko, V V
AU - Makarenko, S V
AU - Baichurin, R I
AU - Berestovitskaya, V. M.
AU - Kovalenko, K S
PY - 2017
DA - 2017/12/01
PB - Pleiades Publishing
SP - 1799-1808
IS - 12
VL - 53
SN - 1070-4280
SN - 1608-3393
ER -
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BibTex (up to 50 authors)
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@article{2017_Pelipko,
author = {V V Pelipko and S V Makarenko and R I Baichurin and V. M. Berestovitskaya and K S Kovalenko},
title = {Alkyl 3-nitroacrylates: Synthesis and reactions with cyclohexane-1,3-diones and Meldrum’s acid},
journal = {Russian Journal of Organic Chemistry},
year = {2017},
volume = {53},
publisher = {Pleiades Publishing},
month = {dec},
url = {https://doi.org/10.1134/s107042801712003x},
number = {12},
pages = {1799--1808},
doi = {10.1134/s107042801712003x}
}
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MLA
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Pelipko, V. V., et al. “Alkyl 3-nitroacrylates: Synthesis and reactions with cyclohexane-1,3-diones and Meldrum’s acid.” Russian Journal of Organic Chemistry, vol. 53, no. 12, Dec. 2017, pp. 1799-1808. https://doi.org/10.1134/s107042801712003x.