Ti–Mg-Catalyzed Carbozincation of N-Benzyl-N-(but-3-en-1-yl)hept-2-yn-1-amine with Et2Zn
Publication type: Journal Article
Publication date: 2024-08-01
scimago Q4
wos Q4
SJR: 0.190
CiteScore: 1.3
Impact factor: 0.9
ISSN: 10704280, 16083393
Abstract
It has been shown for the first time that the Ti-Mg-catalyzed carbozincation reaction of N-benzyl-N-(but-3-en-1-yl)hept-2-yn-1-amine with Et2Zn involves the regio- and stereoselective formation of (Z)-1-benzyl-4-methyl-3-pentylidenepiperidine. The effect of the solvent on the Ti-Mg-catalyzed heterocyclization of N-benzyl-N-(but-3-en-1-yl)hept-2-yn-1-amine was studied. A mechanism of the carbozincation of N-homoallyl-substituted propargylamine with Et2Zn in the presence of catalytic amounts of Ti(O-iPr)4 and EtMgBr has been proposed.
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Gabdullin A. M., Kadikova R. N., Ramazanov I. R. Ti–Mg-Catalyzed Carbozincation of N-Benzyl-N-(but-3-en-1-yl)hept-2-yn-1-amine with Et2Zn // Russian Journal of Organic Chemistry. 2024. Vol. 60. No. 8. pp. 1600-1606.
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Gabdullin A. M., Kadikova R. N., Ramazanov I. R. Ti–Mg-Catalyzed Carbozincation of N-Benzyl-N-(but-3-en-1-yl)hept-2-yn-1-amine with Et2Zn // Russian Journal of Organic Chemistry. 2024. Vol. 60. No. 8. pp. 1600-1606.
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TY - JOUR
DO - 10.1134/s1070428024080049
UR - https://link.springer.com/10.1134/S1070428024080049
TI - Ti–Mg-Catalyzed Carbozincation of N-Benzyl-N-(but-3-en-1-yl)hept-2-yn-1-amine with Et2Zn
T2 - Russian Journal of Organic Chemistry
AU - Gabdullin, A. M.
AU - Kadikova, Rita N.
AU - Ramazanov, Ilfir R
PY - 2024
DA - 2024/08/01
PB - Pleiades Publishing
SP - 1600-1606
IS - 8
VL - 60
SN - 1070-4280
SN - 1608-3393
ER -
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@article{2024_Gabdullin,
author = {A. M. Gabdullin and Rita N. Kadikova and Ilfir R Ramazanov},
title = {Ti–Mg-Catalyzed Carbozincation of N-Benzyl-N-(but-3-en-1-yl)hept-2-yn-1-amine with Et2Zn},
journal = {Russian Journal of Organic Chemistry},
year = {2024},
volume = {60},
publisher = {Pleiades Publishing},
month = {aug},
url = {https://link.springer.com/10.1134/S1070428024080049},
number = {8},
pages = {1600--1606},
doi = {10.1134/s1070428024080049}
}
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Gabdullin, A. M., et al. “Ti–Mg-Catalyzed Carbozincation of N-Benzyl-N-(but-3-en-1-yl)hept-2-yn-1-amine with Et2Zn.” Russian Journal of Organic Chemistry, vol. 60, no. 8, Aug. 2024, pp. 1600-1606. https://link.springer.com/10.1134/S1070428024080049.