Synthesis of 2-amino-8-benzylidene-4-phenyl-3,4,5,6,7,8-hexahydro- and -5,6,7,8-tetrahydroquinazoline derivatives
Publication type: Journal Article
Publication date: 2010-09-09
SJR: —
CiteScore: —
Impact factor: —
ISSN: 00100765, 12126950
General Chemistry
Abstract
Base-catalyzed reaction of 2,6-dibenzylidenecyclohexanone and alkylguanidines gave 2-alkylamino-8-benzylidene-4-phenyl-3,4,5,6,7,8-hexahydroquinazolines IVa-c, which were oxidized to 2-alkylamino-8-benzylidene-4-phenyl-5,6,7,8-tetrahydroquinazolines Va-c. The acylamino (VIa-c, VIIa-d, IXa,b) and diacylamino derivatives (VIIIa,b) of the 2-amino-8-benzylidene-4-pheny]-3,4,5,6,7,8-hexahydroquinazoline (II), 2-amino-8-benzylidene-4-phenyl-5,6,7,8-tetrahydroquinazoline (III) and compounds Va-c have also been prepared. These compounds having the E-configuration were converted into the Z isomers XIIa-e by photoisomerization. The structures were confirmed by spectroscopic methods (IR, 1H NMR, 13C NMR).
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Deli J. et al. Synthesis of 2-amino-8-benzylidene-4-phenyl-3,4,5,6,7,8-hexahydro- and -5,6,7,8-tetrahydroquinazoline derivatives // Collection of Czechoslovak Chemical Communications. 2010. Vol. 50. No. 7. pp. 1602-1610.
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Deli J., Lóránd T., Szabó D., Földesi A., Zschunke A. Synthesis of 2-amino-8-benzylidene-4-phenyl-3,4,5,6,7,8-hexahydro- and -5,6,7,8-tetrahydroquinazoline derivatives // Collection of Czechoslovak Chemical Communications. 2010. Vol. 50. No. 7. pp. 1602-1610.
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TY - JOUR
DO - 10.1135/cccc19851602
UR - https://doi.org/10.1135/cccc19851602
TI - Synthesis of 2-amino-8-benzylidene-4-phenyl-3,4,5,6,7,8-hexahydro- and -5,6,7,8-tetrahydroquinazoline derivatives
T2 - Collection of Czechoslovak Chemical Communications
AU - Deli, J
AU - Lóránd, T
AU - Szabó, D
AU - Földesi, A
AU - Zschunke, A
PY - 2010
DA - 2010/09/09
PB - Institute of Organic Chemistry & Biochemistry
SP - 1602-1610
IS - 7
VL - 50
SN - 0010-0765
SN - 1212-6950
ER -
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@article{2010_Deli,
author = {J Deli and T Lóránd and D Szabó and A Földesi and A Zschunke},
title = {Synthesis of 2-amino-8-benzylidene-4-phenyl-3,4,5,6,7,8-hexahydro- and -5,6,7,8-tetrahydroquinazoline derivatives},
journal = {Collection of Czechoslovak Chemical Communications},
year = {2010},
volume = {50},
publisher = {Institute of Organic Chemistry & Biochemistry},
month = {sep},
url = {https://doi.org/10.1135/cccc19851602},
number = {7},
pages = {1602--1610},
doi = {10.1135/cccc19851602}
}
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Deli, J., et al. “Synthesis of 2-amino-8-benzylidene-4-phenyl-3,4,5,6,7,8-hexahydro- and -5,6,7,8-tetrahydroquinazoline derivatives.” Collection of Czechoslovak Chemical Communications, vol. 50, no. 7, Sep. 2010, pp. 1602-1610. https://doi.org/10.1135/cccc19851602.
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