volume 58 issue 3 pages 619-628

Synthesis of RIA Haptens: 3α,11α-Dihydroxy-5α-pregnan-20-one 11-Hemisuccinate

Publication typeJournal Article
Publication date2003-04-07
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ISSN00100765, 12126950
General Chemistry
Abstract

5α-Pregnane-3α,11α-diol-20-one (XVII) was prepared by hydroxylation of 5α-pregnan-3α-ol-20-one (XVI) by Rhizopus nigricans and by chemical conversion of 11α-hydroxyprogesterone (I). The diol XVII was partially acylated with 2-(trimethylsilyl)ethyl hydrogen succinate and the 11α-succinate XVIII was converted to the target 11α-hemisuccinate XXI.

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GOST Copy
Kasal A., Pásztorová S. Synthesis of RIA Haptens: 3α,11α-Dihydroxy-5α-pregnan-20-one 11-Hemisuccinate // Collection of Czechoslovak Chemical Communications. 2003. Vol. 58. No. 3. pp. 619-628.
GOST all authors (up to 50) Copy
Kasal A., Pásztorová S. Synthesis of RIA Haptens: 3α,11α-Dihydroxy-5α-pregnan-20-one 11-Hemisuccinate // Collection of Czechoslovak Chemical Communications. 2003. Vol. 58. No. 3. pp. 619-628.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1135/cccc19930619
UR - https://doi.org/10.1135/cccc19930619
TI - Synthesis of RIA Haptens: 3α,11α-Dihydroxy-5α-pregnan-20-one 11-Hemisuccinate
T2 - Collection of Czechoslovak Chemical Communications
AU - Kasal, Alexander
AU - Pásztorová, Světlana
PY - 2003
DA - 2003/04/07
PB - Institute of Organic Chemistry & Biochemistry
SP - 619-628
IS - 3
VL - 58
SN - 0010-0765
SN - 1212-6950
ER -
BibTex |
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BibTex (up to 50 authors) Copy
@article{2003_Kasal,
author = {Alexander Kasal and Světlana Pásztorová},
title = {Synthesis of RIA Haptens: 3α,11α-Dihydroxy-5α-pregnan-20-one 11-Hemisuccinate},
journal = {Collection of Czechoslovak Chemical Communications},
year = {2003},
volume = {58},
publisher = {Institute of Organic Chemistry & Biochemistry},
month = {apr},
url = {https://doi.org/10.1135/cccc19930619},
number = {3},
pages = {619--628},
doi = {10.1135/cccc19930619}
}
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Kasal, Alexander, and Světlana Pásztorová. “Synthesis of RIA Haptens: 3α,11α-Dihydroxy-5α-pregnan-20-one 11-Hemisuccinate.” Collection of Czechoslovak Chemical Communications, vol. 58, no. 3, Apr. 2003, pp. 619-628. https://doi.org/10.1135/cccc19930619.