Canadian Journal of Chemistry, volume 58, issue 8, pages 815-822

Synthesis, X-ray structure determination, and formation of 3,4,5-trichloroguaiacol occurring in kraft pulp spent bleach liquors

K Lindström
F Osterberg
F. Österberg
Publication typeJournal Article
Publication date1980-04-15
scimago Q3
SJR0.223
CiteScore1.9
Impact factor1.1
ISSN00084042, 14803291
General Chemistry
Catalysis
Organic Chemistry
Abstract

3,4,5-Trichloroguaiacol, which is formed during bleaching of chemical pulp and shown to bioaccumulate in fish, has been synthesized. The structure of the compound has been determined by means of X-ray analysis. The values of the 13C nmr chemical shifts and melting point differ from those previously reported. A reaction mechanism is suggested for the formation of 3,4,5- and 4,5,6-trichloroguaiacol.

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