Canadian Journal of Chemistry

, том 55 , издание 3 , страницы 421-426

Intermediate stages of the sulfohaloform reaction. Preparation of α-halosulfoxides and sulfinyl chlorides. Oxygen-transfer reactions

Тип публикации: Journal Article

Дата публикации: 1977-02-01

Canadian Science Publishing

Canadian Journal of Chemistry

SCImago Q3

WOS Q4

БС3

SJR: 0.28

CiteScore: 2.1

Impact factor: 1

ISSN: 00084042, 14803291

DOI: 10.1139/v77-062

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General Chemistry

Catalysis

Organic Chemistry

Краткое описание

Details are provided of synthetic routes from dialkyl sulfides to both α-halosulfoxides and sulfinyl chlorides. In the case of the former, oxidation of α-halosulfides to the sulfoxide stage is achieved by chlorine in acetic acid containing controlled amounts of water. Sulfinyl chlorides are prepared by chlorination of α-polyhalosulfoxides in methylene chloride. During investigations into the details of the sulfohaloform reaction, a number of novel redox reactions involving oxygen transfer between sulfur species have been observed and these are presented. They include a reduction of a sulfoxide with thionyl chloride.

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Grossert J. S., Hardstaff W. R., Langler R. F. Intermediate stages of the sulfohaloform reaction. Preparation of α-halosulfoxides and sulfinyl chlorides. Oxygen-transfer reactions // Canadian Journal of Chemistry. 1977. Vol. 55. No. 3. pp. 421-426.

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RIS |

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TY - JOUR

DO - 10.1139/v77-062

UR - https://doi.org/10.1139/v77-062

TI - Intermediate stages of the sulfohaloform reaction. Preparation of α-halosulfoxides and sulfinyl chlorides. Oxygen-transfer reactions

T2 - Canadian Journal of Chemistry

AU - Grossert, J. Stuart

AU - Hardstaff, William R.

AU - Langler, Richard F

PY - 1977

DA - 1977/02/01

PB - Canadian Science Publishing

SP - 421-426

IS - 3

VL - 55

SN - 0008-4042

SN - 1480-3291

ER -

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@article{1977_Grossert,

author = {J. Stuart Grossert and William R. Hardstaff and Richard F Langler},

title = {Intermediate stages of the sulfohaloform reaction. Preparation of α-halosulfoxides and sulfinyl chlorides. Oxygen-transfer reactions},

journal = {Canadian Journal of Chemistry},

year = {1977},

volume = {55},

publisher = {Canadian Science Publishing},

month = {feb},

url = {https://doi.org/10.1139/v77-062},

number = {3},

pages = {421--426},

doi = {10.1139/v77-062}

}

MLA

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MLA Скопировать

Grossert, J. Stuart, et al. “Intermediate stages of the sulfohaloform reaction. Preparation of α-halosulfoxides and sulfinyl chlorides. Oxygen-transfer reactions.” Canadian Journal of Chemistry, vol. 55, no. 3, Feb. 1977, pp. 421-426. https://doi.org/10.1139/v77-062.

Издатель

Canadian Science Publishing

Журнал

Canadian Journal of Chemistry

SCImago Q3

WOS Q4

БС3

SJR

0.28

CiteScore

2.1

Impact factor

ISSN

00084042 (Print)

14803291 (Electronic)

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