Oxford University Press
Chemistry Letters
,  volume 34 ,  issue 10 ,  pages 1448-1449

One-step Synthesis of Aluminum Acetylacetonate from [AlO(OH)]n(Boehmite) in Water

Ryo KATAKURA
, 
Yoshihiro Koide
Publication type: Journal Article
Publication date: 2005-10-01
Oxford University Press
scimago Q3
wos Q4
SJR: 0.374
CiteScore: 2.8
Impact factor: 1.1
ISSN: 03667022, 13480715
General Chemistry
Abstract
Aluminum acetylacetonate, Al(acac) 3 , was prepared in the reaction between the mineral boehmite, [AlO(OH)] n , and acetylacetone (2,4-pentanedione; Hacac) in water. In this one-step synthesis, the pale yellow crystalline product precipitated out of the solution. Characterization of the recrystallized crystal by mass spectrometry, thermogravimetric/differential thermal analysis (TG/DTA), 1 H NMR, and the X-ray diffraction (XRD) was consistent with Al(acac) 3 . This is the first example of the preparation of the six-coordinate aluminum compound from boehmite.
Found 
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KATAKURA R., Koide Y. One-step Synthesis of Aluminum Acetylacetonate from [AlO(OH)]n(Boehmite) in Water // Chemistry Letters. 2005. Vol. 34. No. 10. pp. 1448-1449.
GOST all authors (up to 50) Copy
KATAKURA R., Koide Y. One-step Synthesis of Aluminum Acetylacetonate from [AlO(OH)]n(Boehmite) in Water // Chemistry Letters. 2005. Vol. 34. No. 10. pp. 1448-1449.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1246/cl.2005.1448
UR - https://doi.org/10.1246/cl.2005.1448
TI - One-step Synthesis of Aluminum Acetylacetonate from [AlO(OH)]n(Boehmite) in Water
T2 - Chemistry Letters
AU - KATAKURA, Ryo
AU - Koide, Yoshihiro
PY - 2005
DA - 2005/10/01
PB - Oxford University Press
SP - 1448-1449
IS - 10
VL - 34
SN - 0366-7022
SN - 1348-0715
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2005_KATAKURA,
author = {Ryo KATAKURA and Yoshihiro Koide},
title = {One-step Synthesis of Aluminum Acetylacetonate from [AlO(OH)]n(Boehmite) in Water},
journal = {Chemistry Letters},
year = {2005},
volume = {34},
publisher = {Oxford University Press},
month = {oct},
url = {https://doi.org/10.1246/cl.2005.1448},
number = {10},
pages = {1448--1449},
doi = {10.1246/cl.2005.1448}
}
MLA
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MLA Copy
KATAKURA, Ryo, and Yoshihiro Koide. “One-step Synthesis of Aluminum Acetylacetonate from [AlO(OH)]n(Boehmite) in Water.” Chemistry Letters, vol. 34, no. 10, Oct. 2005, pp. 1448-1449. https://doi.org/10.1246/cl.2005.1448.