The Bond Character of the Sn–Cl Bonds in the Hydrates of Tin (IV) Chloride
Тип публикации: Journal Article
Дата публикации: 1969-09-01
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wos Q2
БС1
SJR: 0.678
CiteScore: 7
Impact factor: 3.8
ISSN: 00092673, 13480634
General Chemistry
Краткое описание
Several hydrates of tin(IV) chloride, e.g., SnCl4·xH2O (x=2, 3, 4 and 5) and SnCl4·yD2O (y=3, 4 and 5), were investigated by means of the nuclear quadrupole resonance (NQR) due to 35Cl and the Mossbauer effect due to 119Sn. The NQR-frequencies were observed at the temperature of liquid nitrogen and room temperature; they were found to range from 17.656 to 21.439 MHz. The Mossbauer effect was investigated only at the temperature of liquid nitrogen; it resulted in isomer shifts ranging from 0.275 to 0.350 mm/sec. The NQR-frequency and the isomer shift decreased with an increase in the number of water molecules in the hydrates, and the relationship between the NQR-frequency and the isomer shift was nearly linear. This relation was interpreted in terms of the transfer of the s-electrons of the tin atom to the chlorine atoms. Furthermore, it was revealed that there was a significant difference between the Sn-Cl bond of the hydrates and that of ammonium chlorostannate.
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Negita H., OKUDA T., Mishima M. The Bond Character of the Sn–Cl Bonds in the Hydrates of Tin (IV) Chloride // Bulletin of the Chemical Society of Japan. 1969. Vol. 42. No. 9. pp. 2509-2513.
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Negita H., OKUDA T., Mishima M. The Bond Character of the Sn–Cl Bonds in the Hydrates of Tin (IV) Chloride // Bulletin of the Chemical Society of Japan. 1969. Vol. 42. No. 9. pp. 2509-2513.
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TY - JOUR
DO - 10.1246/bcsj.42.2509
UR - https://doi.org/10.1246/bcsj.42.2509
TI - The Bond Character of the Sn–Cl Bonds in the Hydrates of Tin (IV) Chloride
T2 - Bulletin of the Chemical Society of Japan
AU - Negita, Hisao
AU - OKUDA, Tsutomu
AU - Mishima, Mitsuo
PY - 1969
DA - 1969/09/01
PB - Oxford University Press
SP - 2509-2513
IS - 9
VL - 42
SN - 0009-2673
SN - 1348-0634
ER -
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@article{1969_Negita,
author = {Hisao Negita and Tsutomu OKUDA and Mitsuo Mishima},
title = {The Bond Character of the Sn–Cl Bonds in the Hydrates of Tin (IV) Chloride},
journal = {Bulletin of the Chemical Society of Japan},
year = {1969},
volume = {42},
publisher = {Oxford University Press},
month = {sep},
url = {https://doi.org/10.1246/bcsj.42.2509},
number = {9},
pages = {2509--2513},
doi = {10.1246/bcsj.42.2509}
}
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Negita, Hisao, et al. “The Bond Character of the Sn–Cl Bonds in the Hydrates of Tin (IV) Chloride.” Bulletin of the Chemical Society of Japan, vol. 42, no. 9, Sep. 1969, pp. 2509-2513. https://doi.org/10.1246/bcsj.42.2509.