Syntheses of 15α-Hydroxyestrone and 15α-Hydroxyestradiol
Publication type: Journal Article
Publication date: 2011-12-08
scimago Q3
wos Q3
SJR: 0.349
CiteScore: 2.7
Impact factor: 1.3
ISSN: 00092363, 13475223
PubMed ID:
1218452
General Chemistry
Drug Discovery
General Medicine
Abstract
The titled compounds (1, 2) have been prepared from estrone by the new synthetic routes. Introduction of a hydroxyl group into the 15α-position was readily attained by hydroboration of the 14, 15-or 15, 16-double bond with diborane and subsequent oxidation of the organoborane with alkaline hydrogen peroxide. In the preparation of 1 the dimethyl-tert-butylsilyl function was conveniently employed for the purpose of protecting the 3, 17β-hydroxyl groups.
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Total citations:
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Citations from 2024:
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GOST
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Hosoda H., YAMASHITA K., Nambara T. Syntheses of 15α-Hydroxyestrone and 15α-Hydroxyestradiol // Chemical and Pharmaceutical Bulletin. 2011. Vol. 23. No. 12. pp. 3141-3145.
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Hosoda H., YAMASHITA K., Nambara T. Syntheses of 15α-Hydroxyestrone and 15α-Hydroxyestradiol // Chemical and Pharmaceutical Bulletin. 2011. Vol. 23. No. 12. pp. 3141-3145.
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RIS
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TY - JOUR
DO - 10.1248/cpb.23.3141
UR - https://doi.org/10.1248/cpb.23.3141
TI - Syntheses of 15α-Hydroxyestrone and 15α-Hydroxyestradiol
T2 - Chemical and Pharmaceutical Bulletin
AU - Hosoda, Hiroshi
AU - YAMASHITA, Kouwa
AU - Nambara, Toshio
PY - 2011
DA - 2011/12/08
PB - Pharmaceutical Society of Japan
SP - 3141-3145
IS - 12
VL - 23
PMID - 1218452
SN - 0009-2363
SN - 1347-5223
ER -
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BibTex (up to 50 authors)
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@article{2011_Hosoda,
author = {Hiroshi Hosoda and Kouwa YAMASHITA and Toshio Nambara},
title = {Syntheses of 15α-Hydroxyestrone and 15α-Hydroxyestradiol},
journal = {Chemical and Pharmaceutical Bulletin},
year = {2011},
volume = {23},
publisher = {Pharmaceutical Society of Japan},
month = {dec},
url = {https://doi.org/10.1248/cpb.23.3141},
number = {12},
pages = {3141--3145},
doi = {10.1248/cpb.23.3141}
}
Cite this
MLA
Copy
Hosoda, Hiroshi, et al. “Syntheses of 15α-Hydroxyestrone and 15α-Hydroxyestradiol.” Chemical and Pharmaceutical Bulletin, vol. 23, no. 12, Dec. 2011, pp. 3141-3145. https://doi.org/10.1248/cpb.23.3141.