Cularine and Related Compounds. V. Investigation of the Ullmann Reaction Products of Methyl (2-Bromo-4, 5-dimethoxyphenyl) acetate with Phenolic Compounds, and an Approach to the Total Synthesis of Cularine.
Тип публикации: Journal Article
Дата публикации: 2011-12-08
SCImago Q3
WOS Q3
БС2
SJR: 0.318
CiteScore: 2.4
Impact factor: 1.5
ISSN: 00092363, 13475223
PubMed ID:
14075283
General Chemistry
Drug Discovery
General Medicine
Краткое описание
Preparation of the cyclic amide (II) as the key intermediate for the synthesis of cularine was elaborated. Bischler-Napieralski cyclization of this amide appeared to proceed as expected to give the desired isoquinoline derivative, didehydronorcularine, in a crude state, which, however, was readily oxidized and turned during purification into the corresponding ketone derivative, which was characterized as its picrate.
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Kametani T. et al. Cularine and Related Compounds. V. Investigation of the Ullmann Reaction Products of Methyl (2-Bromo-4, 5-dimethoxyphenyl) acetate with Phenolic Compounds, and an Approach to the Total Synthesis of Cularine. // Chemical and Pharmaceutical Bulletin. 2011. Vol. 11. No. 10. pp. 1299-1305.
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Kametani T., FUKUMOTO K., SHIBUYA S., Nakano T. Cularine and Related Compounds. V. Investigation of the Ullmann Reaction Products of Methyl (2-Bromo-4, 5-dimethoxyphenyl) acetate with Phenolic Compounds, and an Approach to the Total Synthesis of Cularine. // Chemical and Pharmaceutical Bulletin. 2011. Vol. 11. No. 10. pp. 1299-1305.
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TY - JOUR
DO - 10.1248/cpb.11.1299
UR - https://doi.org/10.1248/cpb.11.1299
TI - Cularine and Related Compounds. V. Investigation of the Ullmann Reaction Products of Methyl (2-Bromo-4, 5-dimethoxyphenyl) acetate with Phenolic Compounds, and an Approach to the Total Synthesis of Cularine.
T2 - Chemical and Pharmaceutical Bulletin
AU - Kametani, Tetsuji
AU - FUKUMOTO, Keiichiro
AU - SHIBUYA, Shiroshi
AU - Nakano, Takuo
PY - 2011
DA - 2011/12/08
PB - Pharmaceutical Society of Japan
SP - 1299-1305
IS - 10
VL - 11
PMID - 14075283
SN - 0009-2363
SN - 1347-5223
ER -
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@article{2011_Kametani,
author = {Tetsuji Kametani and Keiichiro FUKUMOTO and Shiroshi SHIBUYA and Takuo Nakano},
title = {Cularine and Related Compounds. V. Investigation of the Ullmann Reaction Products of Methyl (2-Bromo-4, 5-dimethoxyphenyl) acetate with Phenolic Compounds, and an Approach to the Total Synthesis of Cularine.},
journal = {Chemical and Pharmaceutical Bulletin},
year = {2011},
volume = {11},
publisher = {Pharmaceutical Society of Japan},
month = {dec},
url = {https://doi.org/10.1248/cpb.11.1299},
number = {10},
pages = {1299--1305},
doi = {10.1248/cpb.11.1299}
}
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Kametani, Tetsuji, et al. “Cularine and Related Compounds. V. Investigation of the Ullmann Reaction Products of Methyl (2-Bromo-4, 5-dimethoxyphenyl) acetate with Phenolic Compounds, and an Approach to the Total Synthesis of Cularine..” Chemical and Pharmaceutical Bulletin, vol. 11, no. 10, Dec. 2011, pp. 1299-1305. https://doi.org/10.1248/cpb.11.1299.
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