On the Benzylation of Nucleosides. I. Reaction of Uridine with Benzyl Bromide in the Presence of Sodium Hydride
Тип публикации: Journal Article
Дата публикации: 2011-12-08
SCImago Q3
WOS Q3
БС2
SJR: 0.318
CiteScore: 2.4
Impact factor: 1.5
ISSN: 00092363, 13475223
PubMed ID:
5706820
General Chemistry
Drug Discovery
General Medicine
Краткое описание
Uridine was benzylated with benzyl bromide in the presence of sodium hydride in dimethyl sulfoxide or dimethylformamide to give two products. The one was a dibenzyl uridine (I), yield 33%, and the other N3-benzyluridine (II), yield 30.5%. The product (I) was converted to the product (II) by catalytic hydrogenation and was identified with N3, 2'-O-dibenzyluridine which was synthesized by detritylation of N3, 2'-O-dibenzyl-3', 5'-di-O-trityluridine (IV) derived by the similar benzylation of the known 3', 5'-di-O-trityluridine (III).
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IMURA N., TSURUO T., UKITA T. On the Benzylation of Nucleosides. I. Reaction of Uridine with Benzyl Bromide in the Presence of Sodium Hydride // Chemical and Pharmaceutical Bulletin. 2011. Vol. 16. No. 6. pp. 1105-1109.
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IMURA N., TSURUO T., UKITA T. On the Benzylation of Nucleosides. I. Reaction of Uridine with Benzyl Bromide in the Presence of Sodium Hydride // Chemical and Pharmaceutical Bulletin. 2011. Vol. 16. No. 6. pp. 1105-1109.
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TY - JOUR
DO - 10.1248/cpb.16.1105
UR - https://doi.org/10.1248/cpb.16.1105
TI - On the Benzylation of Nucleosides. I. Reaction of Uridine with Benzyl Bromide in the Presence of Sodium Hydride
T2 - Chemical and Pharmaceutical Bulletin
AU - IMURA, NOBUMASA
AU - TSURUO, Takashi
AU - UKITA, Tyunosin
PY - 2011
DA - 2011/12/08
PB - Pharmaceutical Society of Japan
SP - 1105-1109
IS - 6
VL - 16
PMID - 5706820
SN - 0009-2363
SN - 1347-5223
ER -
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BibTex (до 50 авторов)
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@article{2011_IMURA,
author = {NOBUMASA IMURA and Takashi TSURUO and Tyunosin UKITA},
title = {On the Benzylation of Nucleosides. I. Reaction of Uridine with Benzyl Bromide in the Presence of Sodium Hydride},
journal = {Chemical and Pharmaceutical Bulletin},
year = {2011},
volume = {16},
publisher = {Pharmaceutical Society of Japan},
month = {dec},
url = {https://doi.org/10.1248/cpb.16.1105},
number = {6},
pages = {1105--1109},
doi = {10.1248/cpb.16.1105}
}
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MLA
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IMURA, NOBUMASA, et al. “On the Benzylation of Nucleosides. I. Reaction of Uridine with Benzyl Bromide in the Presence of Sodium Hydride.” Chemical and Pharmaceutical Bulletin, vol. 16, no. 6, Dec. 2011, pp. 1105-1109. https://doi.org/10.1248/cpb.16.1105.
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