Pure and Applied Chemistry

, том 90 , издание 1 , страницы 7-20

Silica gel mediated oxidative C–O coupling of β-dicarbonyl compounds with malonyl peroxides in solvent-free conditions

Тип публикации: Journal Article

Дата публикации: 2017-05-24

Walter de Gruyter

Pure and Applied Chemistry

scimago Q2

wos Q3

БС2

SJR: 0.426

CiteScore: 3.2

Impact factor: 2.0

ISSN: 00334545, 13653075

DOI: 10.1515/pac-2017-0312

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General Chemistry

General Chemical Engineering

Краткое описание

For the first time silica gel was observed to activate peroxides in oxidative coupling reactions. Here we report silica gel mediated oxidative C–O coupling of β-dicarbonyl compounds with cyclic diacyl peroxides affording α-acyloxy derivatives with 100% atom efficiency. The highest yields of coupling products were achieved in solvent free conditions. C–O coupling products were prepared in yields up to 86%.

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Bityukov O. V. et al. Silica gel mediated oxidative C–O coupling of β-dicarbonyl compounds with malonyl peroxides in solvent-free conditions // Pure and Applied Chemistry. 2017. Vol. 90. No. 1. pp. 7-20.

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Bityukov O. V., Vil’ V. A., Merkulova V. M., Nikishin G. I., Terent'ev A. O. Silica gel mediated oxidative C–O coupling of β-dicarbonyl compounds with malonyl peroxides in solvent-free conditions // Pure and Applied Chemistry. 2017. Vol. 90. No. 1. pp. 7-20.

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TY - JOUR

DO - 10.1515/pac-2017-0312

UR - https://www.degruyter.com/document/doi/10.1515/pac-2017-0312/html

TI - Silica gel mediated oxidative C–O coupling of β-dicarbonyl compounds with malonyl peroxides in solvent-free conditions

T2 - Pure and Applied Chemistry

AU - Bityukov, Oleg V

AU - Vil’, Vera A.

AU - Merkulova, Valentina M

AU - Nikishin, Gennady I.

AU - Terent'ev, Alexander O.

PY - 2017

DA - 2017/05/24

PB - Walter de Gruyter

SP - 7-20

IS - 1

VL - 90

SN - 0033-4545

SN - 1365-3075

ER -

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@article{2017_Bityukov,

author = {Oleg V Bityukov and Vera A. Vil’ and Valentina M Merkulova and Gennady I. Nikishin and Alexander O. Terent'ev},

title = {Silica gel mediated oxidative C–O coupling of β-dicarbonyl compounds with malonyl peroxides in solvent-free conditions},

journal = {Pure and Applied Chemistry},

year = {2017},

volume = {90},

publisher = {Walter de Gruyter},

month = {may},

url = {https://www.degruyter.com/document/doi/10.1515/pac-2017-0312/html},

number = {1},

pages = {7--20},

doi = {10.1515/pac-2017-0312}

}

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Bityukov, Oleg V., et al. “Silica gel mediated oxidative C–O coupling of β-dicarbonyl compounds with malonyl peroxides in solvent-free conditions.” Pure and Applied Chemistry, vol. 90, no. 1, May. 2017, pp. 7-20. https://www.degruyter.com/document/doi/10.1515/pac-2017-0312/html.

Издатель

Walter de Gruyter

Журнал

Pure and Applied Chemistry

scimago Q2

wos Q3

БС2

SJR

0.426

CiteScore

3.2

Impact factor

2.0

ISSN

00334545 (Print)

13653075 (Electronic)

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