Walter de Gruyter
Zeitschrift fur Kristallographie - Crystalline Materials
,  volume 234 ,  issue 2 ,  pages 109-118

Open-framework sodium uranyl selenate and sodium uranyl sulfate with protonated morpholino-N-acetic acid

Oleg I Siidra 1, 2
, 
Evgeny V. Nazarchuk 1
, 
Dmitry O. Charkin 3
, 
Nikita V. Chukanov 4
, 
Alexander Yu. Zakharov 3
, 
Stepan N. Kalmykov 3
, 
Yuriy A Ikhalaynen 3
, 
Mikhail I Sharikov 3
1
 
2
 
3
 
4
 
Publication type: Journal Article
Publication date: 2018-09-27
Walter de Gruyter
SJR: —
CiteScore: —
Impact factor: —
ISSN: 21944946, 21967105
Inorganic Chemistry
Condensed Matter Physics
General Materials Science
Abstract

The reaction of sodium N-morpholine acetate with selenic and sulfuric acid and uranyl nitrate results in the formation of two novel open-framework compounds, |Na(Hmfa)|[(UO2)2(SeO4)3(H2O)](H2O)2 (NaUSe) and [Na2(SO3OH)(Hmfa)]|(UO2)(SO4)2| (NaUS), respectively. Despite identical synthetic procedures, sulfate structure dramatically differs from selenate compound. Their common feature is an open-framework featuring two-dimensional system of channels occupied by protonated morpholino-N-acetic acid species. Coordination of Na atoms is different. In NaUSe, [(UO2)2 (SeO4)3(H2O)]2− layers are pillared by {Na2O8(H2O)2(Hmfa)2} complexes to form a microporous framework. In NaUS, UO7 and SO4 polyhedra of [(UO2)(SO4)2]2− chains share common oxygen atoms with Na-centered tetrameric complexes providing a three-dimensional integrity of the structure. Both of the compounds are characterized by IR spectroscopy.

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Siidra O. I. et al. Open-framework sodium uranyl selenate and sodium uranyl sulfate with protonated morpholino-N-acetic acid // Zeitschrift fur Kristallographie - Crystalline Materials. 2018. Vol. 234. No. 2. pp. 109-118.
GOST all authors (up to 50) Copy
Siidra O. I., Nazarchuk E. V., Charkin D. O., Chukanov N. V., Zakharov A. Y., Kalmykov S. N., Ikhalaynen Y. A., Sharikov M. I. Open-framework sodium uranyl selenate and sodium uranyl sulfate with protonated morpholino-N-acetic acid // Zeitschrift fur Kristallographie - Crystalline Materials. 2018. Vol. 234. No. 2. pp. 109-118.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1515/zkri-2018-2103
UR - https://doi.org/10.1515/zkri-2018-2103
TI - Open-framework sodium uranyl selenate and sodium uranyl sulfate with protonated morpholino-N-acetic acid
T2 - Zeitschrift fur Kristallographie - Crystalline Materials
AU - Siidra, Oleg I
AU - Nazarchuk, Evgeny V.
AU - Charkin, Dmitry O.
AU - Chukanov, Nikita V.
AU - Zakharov, Alexander Yu.
AU - Kalmykov, Stepan N.
AU - Ikhalaynen, Yuriy A
AU - Sharikov, Mikhail I
PY - 2018
DA - 2018/09/27
PB - Walter de Gruyter
SP - 109-118
IS - 2
VL - 234
SN - 2194-4946
SN - 2196-7105
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2018_Siidra,
author = {Oleg I Siidra and Evgeny V. Nazarchuk and Dmitry O. Charkin and Nikita V. Chukanov and Alexander Yu. Zakharov and Stepan N. Kalmykov and Yuriy A Ikhalaynen and Mikhail I Sharikov},
title = {Open-framework sodium uranyl selenate and sodium uranyl sulfate with protonated morpholino-N-acetic acid},
journal = {Zeitschrift fur Kristallographie - Crystalline Materials},
year = {2018},
volume = {234},
publisher = {Walter de Gruyter},
month = {sep},
url = {https://doi.org/10.1515/zkri-2018-2103},
number = {2},
pages = {109--118},
doi = {10.1515/zkri-2018-2103}
}
MLA
Cite this
MLA Copy
Siidra, Oleg I., et al. “Open-framework sodium uranyl selenate and sodium uranyl sulfate with protonated morpholino-N-acetic acid.” Zeitschrift fur Kristallographie - Crystalline Materials, vol. 234, no. 2, Sep. 2018, pp. 109-118. https://doi.org/10.1515/zkri-2018-2103.