,
volume 44
,
issue 10
,
pages 1239-1246
Das System Pyridin-Chlorwasserstoff: Bildung und Struktur kristalliner Addukte / The System Pyridine-Hydrogen Chloride: Formation and Structure of Crystalline Adducts
Publication type: Journal Article
Publication date: 1989-10-01
scimago Q3
wos Q4
SJR: 0.259
CiteScore: 1.5
Impact factor: 0.8
ISSN: 09320776, 18657117
General Chemistry
Abstract
The melting diagram of the system pyridine-hydrogen chloride was determined by DTA. It reveals the existence of intermediary solid complexes pyridine · xHCl with x = 0.5, 1, 2, 4 and 6. The structures of those with x = 1 (room-temperature phase), 2, 4 and 6 were determined from single-crystal MoKa diffractometer data at low temperatures. Pyridinium and chloride ions and, with the exception of the mono-adduct, hydrogen chloride molecules are hydrogen-bonded into various discrete molecular and complex-ionic structural units. Among these are the first poly-(hydrogen chloride) anions, HnCln+1 - or [Cl(HCl)n]- with n > 1 (viz. n = 2, 4 and 5), characterized by crystal structure analysis.
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Mootz D., Hocken J. Das System Pyridin-Chlorwasserstoff: Bildung und Struktur kristalliner Addukte / The System Pyridine-Hydrogen Chloride: Formation and Structure of Crystalline Adducts // Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences. 1989. Vol. 44. No. 10. pp. 1239-1246.
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Mootz D., Hocken J. Das System Pyridin-Chlorwasserstoff: Bildung und Struktur kristalliner Addukte / The System Pyridine-Hydrogen Chloride: Formation and Structure of Crystalline Adducts // Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences. 1989. Vol. 44. No. 10. pp. 1239-1246.
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RIS
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TY - JOUR
DO - 10.1515/znb-1989-1017
UR - https://doi.org/10.1515/znb-1989-1017
TI - Das System Pyridin-Chlorwasserstoff: Bildung und Struktur kristalliner Addukte / The System Pyridine-Hydrogen Chloride: Formation and Structure of Crystalline Adducts
T2 - Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences
AU - Mootz, Dietrich
AU - Hocken, Jörg
PY - 1989
DA - 1989/10/01
PB - Walter de Gruyter
SP - 1239-1246
IS - 10
VL - 44
SN - 0932-0776
SN - 1865-7117
ER -
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@article{1989_Mootz,
author = {Dietrich Mootz and Jörg Hocken},
title = {Das System Pyridin-Chlorwasserstoff: Bildung und Struktur kristalliner Addukte / The System Pyridine-Hydrogen Chloride: Formation and Structure of Crystalline Adducts},
journal = {Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences},
year = {1989},
volume = {44},
publisher = {Walter de Gruyter},
month = {oct},
url = {https://doi.org/10.1515/znb-1989-1017},
number = {10},
pages = {1239--1246},
doi = {10.1515/znb-1989-1017}
}
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Mootz, Dietrich, and Jörg Hocken. “Das System Pyridin-Chlorwasserstoff: Bildung und Struktur kristalliner Addukte / The System Pyridine-Hydrogen Chloride: Formation and Structure of Crystalline Adducts.” Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, vol. 44, no. 10, Oct. 1989, pp. 1239-1246. https://doi.org/10.1515/znb-1989-1017.