Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, volume 50, issue 6, pages 905-912

The Ternary Rare Earth Chromium Nitrides Ce₂CrN₃ and Ln₃Cr_10−xN₁₁ with Ln = La, Ce, Pr

Sascha Broil ¹

Wolfgang Jeitschko ¹

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Anorganisch-Chemisches Institut, Universität Münster, Wilhelm -Klemm -Straße 8, D-48149 Münster, Germany |

Publication type: Journal Article

Publication date: 1995-06-01

Walter de Gruyter

Journal: Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

Quartile SCImago

Quartile WOS

Impact factor: 0.8

ISSN: 09320776

DOI: 10.1515/znb-1995-0612

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General Chemistry

Abstract

The title compounds have been prepared by annealing cold-pressed pellets of the binary nitrides LnN and CrN. Well developed crystals were obtained by recrystallization of the binary or prereacted ternary nitrides in a Li₃N flux. Their structures were determined from single-crystal diffractometer data. C e₂CrN₃ has a U₂CrN₃ type structure: Immm , a = 379.0(1), b = 340.4(1), c = 1251.7(2) pm, Z = 2, R = 0.012 for 383 structure factors and 16 variables. The atomic positions of this structure are similar to those of U₂IrC₂ and K₂NiF₄. The structure may be rationalized to a first approximation with the formula (Ce⁺⁴)₂[CrN₃]⁸⁻. The chromium atoms are in a distorted square-planar nitrogen coordination. The CrN₄-squares are linked via corner-sharing nitrogen atoms, thus forming infinite, straight - N - CrN₂- N - CrN₂- chains. The cubic structure of La₃Cr_10−xN₁₁ (a = 1298.2(1) pm ), Ce₃Cr_10−xN₁₁ (with a small homogenity range; a = 1284.3(1)-1286.1(3) pm ), and Pr₃Cr_10−xN₁₁ (a = 1289.1(2) pm ) was determined for the lanthanum compound: Fm 3̄ m , Z = 8, R = 0.027 for 189 F values and 18 variables. One chromium site was found to have an occupancy of only 80.9(5)% resulting in the composition La₃Cr_9.24(1)N₁₁. The nitrogen atoms occupy four atomic sites. Three of these have octahedral environments (6 La, 3 La + 3 Cr, 2 La + 4 Cr), the fourth one is surrounded by eight chromium atoms forming a cube. The chromium atoms are tetrahedrally coordinated by nitrogen atoms, and these CrN₄-tetrahedra are linked via common corners and edges to form a three-dimensionally infinite polyanionic network. In addition the chromium atoms with oxidation numbers of about 2 to 3 form numerous Cr - Cr bonds, which allow to rationalize the Pauli paramagnetism of the compound.

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Elsevier	Elsevier, 8, 20.51% Elsevier 8 publications, 20.51%
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Broil S., Jeitschko W. The Ternary Rare Earth Chromium Nitrides Ce2CrN3 and Ln3Cr10−xN11 with Ln = La, Ce, Pr // Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences. 1995. Vol. 50. No. 6. pp. 905-912.

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TY - JOUR

DO - 10.1515/znb-1995-0612

UR - https://doi.org/10.1515/znb-1995-0612

TI - The Ternary Rare Earth Chromium Nitrides Ce2CrN3 and Ln3Cr10−xN11 with Ln = La, Ce, Pr

T2 - Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

AU - Broil, Sascha

AU - Jeitschko, Wolfgang

PY - 1995

DA - 1995/06/01 00:00:00

PB - Walter de Gruyter

SP - 905-912

IS - 6

VL - 50

SN - 0932-0776

ER -

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@article{1995_Broil,

author = {Sascha Broil and Wolfgang Jeitschko},

title = {The Ternary Rare Earth Chromium Nitrides Ce2CrN3 and Ln3Cr10−xN11 with Ln = La, Ce, Pr},

journal = {Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences},

year = {1995},

volume = {50},

publisher = {Walter de Gruyter},

month = {jun},

url = {https://doi.org/10.1515/znb-1995-0612},

number = {6},

pages = {905--912},

doi = {10.1515/znb-1995-0612}

}

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Broil, Sascha, and Wolfgang Jeitschko. “The Ternary Rare Earth Chromium Nitrides Ce2CrN3 and Ln3Cr10−xN11 with Ln = La, Ce, Pr.” Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, vol. 50, no. 6, Jun. 1995, pp. 905-912. https://doi.org/10.1515/znb-1995-0612.

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Publisher

Walter de Gruyter

Journal

Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

Quartile SCImago

Quartile WOS

Impact factor

0.8

ISSN

09320776 (Print)