Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

, volume 53 , issue 11 , pages 1247-1254

9-Silyl(-Germyl,-Stannyl) Substituted Derivatives of 1-(9-Fluorenyl)-germatranes. Synthesis, Characterisation, and Crystal Structures

Galina S. Zaitseva ¹

Sergey S. Karlov ¹

Bettina A Siggelkow ²

Evgeni V Avtomonov ²

Andrei V. Churakov ³

Judith A. K. Howard ³

Jörg Lorberth ²

Hide authors affiliations Show authors affiliations: 3 affiliations

Chemistry Department, Moscow State University, B-234 Vorob’evy Gory, 119899 Moscow, Russia |

Fachbereich Chemie, Philipps-Universität Marburg, Hans-Meerwein-Straße, D-35032 Marburg / Lahn, Germany |

Department of Chemistry, University of Durham, Science Laboratories, South Road, Durham, DH1 3LE, England |

Publication type: Journal Article

Publication date: 1998-11-01

Walter de Gruyter

Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

scimago Q3

wos Q4

SJR: 0.259

CiteScore: 1.5

Impact factor: 0.8

ISSN: 09320776, 18657117

DOI: 10.1515/znb-1998-1101

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General Chemistry

Abstract

9-Trimethylsilyl- and 9-trimethylgermyl substituted derivatives of 1-(9-fluorenyl)germatranes C₁₃H₈(R)Ge(OCH₂CH₂)₃N (1 - 3) (1: R = H; 2: R = Me₃Si; 3: R = Me₃Ge) were prepared by the reaction of 9-tribromogermyl derivatives of fluorene C₁₃H₈(R)GeBr₃ (4 - 6) with N(CH₂CH₂OSnAlk₃)₃ (7: Alk = Et; 8: Alk = Bu). 1-(9-Trimethylstannyl- 9-fluorenyl)germatrane (14) was synthesised by the reaction o f the germatrane (1) with Me₃SnNMe₂ . Formulas and structures were established by elemental analyses, (¹H, ¹³C) NMR spectroscopy and mass spectrometry; crystal structures of 2 and 14 are reported.

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Churakov Andrei

PhD in Chemistry

555 publications, 7 064 citations, 14 reviews

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Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

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Tyurin Daniil

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PhD in Chemistry

73 publications, 687 citations

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Lomonosov Moscow State University

Computational chemistry

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Interaction of X-ray and synchrotron radiation with matter

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Molecular modeling

Molecular spectroscopy

Non-covalent Interactions

Non-valent interactions

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Zaitseva G. S. et al. 9-Silyl(-Germyl,-Stannyl) Substituted Derivatives of 1-(9-Fluorenyl)-germatranes. Synthesis, Characterisation, and Crystal Structures // Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences. 1998. Vol. 53. No. 11. pp. 1247-1254.

GOST all authors (up to 50) Copy

Zaitseva G. S., Karlov S. S., Siggelkow B. A., Avtomonov E. V., Churakov A. V., Howard J. A. K., Lorberth J. 9-Silyl(-Germyl,-Stannyl) Substituted Derivatives of 1-(9-Fluorenyl)-germatranes. Synthesis, Characterisation, and Crystal Structures // Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences. 1998. Vol. 53. No. 11. pp. 1247-1254.

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RIS Copy

TY - JOUR

DO - 10.1515/znb-1998-1101

UR - https://www.degruyter.com/document/doi/10.1515/znb-1998-1101/html

TI - 9-Silyl(-Germyl,-Stannyl) Substituted Derivatives of 1-(9-Fluorenyl)-germatranes. Synthesis, Characterisation, and Crystal Structures

T2 - Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

AU - Zaitseva, Galina S.

AU - Karlov, Sergey S.

AU - Siggelkow, Bettina A

AU - Avtomonov, Evgeni V

AU - Churakov, Andrei V.

AU - Howard, Judith A. K.

AU - Lorberth, Jörg

PY - 1998

DA - 1998/11/01

PB - Walter de Gruyter

SP - 1247-1254

IS - 11

VL - 53

SN - 0932-0776

SN - 1865-7117

ER -

BibTex |

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@article{1998_Zaitseva,

author = {Galina S. Zaitseva and Sergey S. Karlov and Bettina A Siggelkow and Evgeni V Avtomonov and Andrei V. Churakov and Judith A. K. Howard and Jörg Lorberth},

title = {9-Silyl(-Germyl,-Stannyl) Substituted Derivatives of 1-(9-Fluorenyl)-germatranes. Synthesis, Characterisation, and Crystal Structures},

journal = {Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences},

year = {1998},

volume = {53},

publisher = {Walter de Gruyter},

month = {nov},

url = {https://www.degruyter.com/document/doi/10.1515/znb-1998-1101/html},

number = {11},

pages = {1247--1254},

doi = {10.1515/znb-1998-1101}

}

MLA

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Zaitseva, Galina S., et al. “9-Silyl(-Germyl,-Stannyl) Substituted Derivatives of 1-(9-Fluorenyl)-germatranes. Synthesis, Characterisation, and Crystal Structures.” Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, vol. 53, no. 11, Nov. 1998, pp. 1247-1254. https://www.degruyter.com/document/doi/10.1515/znb-1998-1101/html.