,
volume 58
,
issue 12
,
pages 1165-1170
Synthesis and Characterization of N-Methyl-Substituted Germocanes. Crystal Structure of MeN(CH2 CH2 O)2 GeBr2
Sergey S. Karlov
1
,
Elmira Kh. Yakubova
1
,
Ekaterina V. Gauchenova
2
,
Anastasia A. Selina
1
,
Judith A. K. Howard
3
,
Daniil A Tyurin
1
,
Jörg Lorberth
2
,
Galina S. Zaitseva
1
Publication type: Journal Article
Publication date: 2003-12-01
scimago Q3
wos Q4
SJR: 0.259
CiteScore: 1.5
Impact factor: 0.8
ISSN: 09320776, 18657117
General Chemistry
Abstract
The reaction of GeHal4 with MeN(CH2CH2OSiMe3)2 affords dihalogermocanes MeN(CH2 CH2O)2GeHal2 (1, Hal = Br; 2, Hal = Cl). Treatment of Me2Ge(NMe2)2 with MeN(CH2CH2OH)2 leads to dimethylgermocane MeN(CH2CH2O)2GeMe2 (3). The composition and structure of 1-3 were established by elemental analyses, 1H, 13C NMR spectroscopy, and mass spectrometry. The crystal structure of 1 is reported; structural data obtained from geometry DFT optimization on 1 are in good agreement with experimental results. Values of the electron density in the N→Ge bond critical point and the Laplacian of charge density for 1-3 indicate a closed-shell interaction between the Ge and N atoms.
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Karlov S. S. et al. Synthesis and Characterization of N-Methyl-Substituted Germocanes. Crystal Structure of MeN(CH2CH2O)2GeBr2 // Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences. 2003. Vol. 58. No. 12. pp. 1165-1170.
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Karlov S. S., Yakubova E. K., Gauchenova E. V., Selina A. A., Churakov A. V., Howard J. A. K., Tyurin D. A., Lorberth J., Zaitseva G. S. Synthesis and Characterization of N-Methyl-Substituted Germocanes. Crystal Structure of MeN(CH2CH2O)2GeBr2 // Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences. 2003. Vol. 58. No. 12. pp. 1165-1170.
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RIS
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TY - JOUR
DO - 10.1515/znb-2003-1203
UR - https://www.degruyter.com/document/doi/10.1515/znb-2003-1203/html
TI - Synthesis and Characterization of N-Methyl-Substituted Germocanes. Crystal Structure of MeN(CH2CH2O)2GeBr2
T2 - Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences
AU - Karlov, Sergey S.
AU - Yakubova, Elmira Kh.
AU - Gauchenova, Ekaterina V.
AU - Selina, Anastasia A.
AU - Churakov, Andrei V.
AU - Howard, Judith A. K.
AU - Tyurin, Daniil A
AU - Lorberth, Jörg
AU - Zaitseva, Galina S.
PY - 2003
DA - 2003/12/01
PB - Walter de Gruyter
SP - 1165-1170
IS - 12
VL - 58
SN - 0932-0776
SN - 1865-7117
ER -
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BibTex (up to 50 authors)
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@article{2003_Karlov,
author = {Sergey S. Karlov and Elmira Kh. Yakubova and Ekaterina V. Gauchenova and Anastasia A. Selina and Andrei V. Churakov and Judith A. K. Howard and Daniil A Tyurin and Jörg Lorberth and Galina S. Zaitseva},
title = {Synthesis and Characterization of N-Methyl-Substituted Germocanes. Crystal Structure of MeN(CH2CH2O)2GeBr2},
journal = {Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences},
year = {2003},
volume = {58},
publisher = {Walter de Gruyter},
month = {dec},
url = {https://www.degruyter.com/document/doi/10.1515/znb-2003-1203/html},
number = {12},
pages = {1165--1170},
doi = {10.1515/znb-2003-1203}
}
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MLA
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Karlov, Sergey S., et al. “Synthesis and Characterization of N-Methyl-Substituted Germocanes. Crystal Structure of MeN(CH2CH2O)2GeBr2.” Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, vol. 58, no. 12, Dec. 2003, pp. 1165-1170. https://www.degruyter.com/document/doi/10.1515/znb-2003-1203/html.
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