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Superheated Water Chromatography of Phenols Using Poly(styrene-divinylbenzene) Packings as a Stationary Phase.
Тип публикации: Journal Article
Дата публикации: 2003-02-01
scimago Q3
wos Q3
БС3
SJR: 0.335
CiteScore: 3.2
Impact factor: 2
ISSN: 09106340, 13482246
PubMed ID:
12608758
Analytical Chemistry
Краткое описание
A method for the superheated water chromatography of phenols was developed using a poly(styrene-divinylbenzene) (PSDVB) stationary phase. The stationary phase of superheated water chromatography must be stable against the attack of water. A durability test for PSDVB packings and octadecylsilyl (ODS)-silica gels indicated that PSDVB packings were stable in superheated water in the temperature range of 100 - 150°C, whereas octadecylsilyl groups of ODS-silica gels cleaved even at 100°C. The retention of phenols on the PSDVB stationary phase decreased with an elevation of the column temperature. The retention mechanism was characterized using a thermodynamic theory that has been used for describing retention in conventional RP-HPLC. The application of the present method to an environmental analysis was also demonstrated, in which a suitable separation with good peak shape was obtained for p-chlorophenol in river-water samples.
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Yarita T., Nakajima R., Shibukawa M. Superheated Water Chromatography of Phenols Using Poly(styrene-divinylbenzene) Packings as a Stationary Phase. // Analytical Sciences. 2003. Vol. 19. No. 2. pp. 269-272.
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Yarita T., Nakajima R., Shibukawa M. Superheated Water Chromatography of Phenols Using Poly(styrene-divinylbenzene) Packings as a Stationary Phase. // Analytical Sciences. 2003. Vol. 19. No. 2. pp. 269-272.
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TY - JOUR
DO - 10.2116/analsci.19.269
UR - https://doi.org/10.2116/analsci.19.269
TI - Superheated Water Chromatography of Phenols Using Poly(styrene-divinylbenzene) Packings as a Stationary Phase.
T2 - Analytical Sciences
AU - Yarita, Takashi
AU - Nakajima, Ryoji
AU - Shibukawa, Masami
PY - 2003
DA - 2003/02/01
PB - Japan Society for Analytical Chemistry
SP - 269-272
IS - 2
VL - 19
PMID - 12608758
SN - 0910-6340
SN - 1348-2246
ER -
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@article{2003_Yarita,
author = {Takashi Yarita and Ryoji Nakajima and Masami Shibukawa},
title = {Superheated Water Chromatography of Phenols Using Poly(styrene-divinylbenzene) Packings as a Stationary Phase.},
journal = {Analytical Sciences},
year = {2003},
volume = {19},
publisher = {Japan Society for Analytical Chemistry},
month = {feb},
url = {https://doi.org/10.2116/analsci.19.269},
number = {2},
pages = {269--272},
doi = {10.2116/analsci.19.269}
}
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Yarita, Takashi, et al. “Superheated Water Chromatography of Phenols Using Poly(styrene-divinylbenzene) Packings as a Stationary Phase..” Analytical Sciences, vol. 19, no. 2, Feb. 2003, pp. 269-272. https://doi.org/10.2116/analsci.19.269.