Synthesis of Formylphenyl 1-Oxo-1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole-7-carboxylates and Their (E)-1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazole-4-yliminomethyl Derivatives
E A Dikusar
1
,
E A Akishina
1
,
N A Zhukouskaya
1
,
I A Kolesnik
1
,
E. N. Margun
1
,
S. S. Kovalskaya
1
,
K. A. Alekseeva
2
,
N. A. Logvinenko
2
,
Daria Menshikova
2
,
Vladimir I. Potkin
1
Publication type: Journal Article
Publication date: 2024-12-20
SJR: —
CiteScore: —
Impact factor: —
ISSN: 0044460X
Abstract
Formylphenyloxohydroepoxyisoindole carboxylates were prepared by the reaction of 4-hydroxy-3-methoxy-, 4-hydroxy-3-ethoxy- and 3-hydroxy-4-methoxybenzaldehydes with substituted isoindolecarboxylic acids {2-methyl-1-oxo-1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole-7-carboxylic, 2-(3,4-dimethoxyphenethyl)1-oxo-1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole-7-carboxylic, 2-(benzo[d][1,3]dioxol-5-ylmethyl)-1-oxo1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole-7-carboxylic, 6-oxo-3,4,6,6a,7,8-hexahydro-2H,10bH-8,10a-epoxy[1,3]oxazino[2,3-a]isoindole-7-carboxylic, 2-(2,3-dichlorobenzyl)-1-oxo-1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole-7-carboxylic} in dichloromethane in the presence of dicyclohexylcarbodiimide. The corresponding (E)-azomethines were synthesized by condensation of formylphenyloxohydroepoxyisoindole carboxylates with 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one in methanol.
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Dikusar E. A. et al. Synthesis of Formylphenyl 1-Oxo-1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole-7-carboxylates and Their (E)-1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazole-4-yliminomethyl Derivatives // Журнал Общей Химии. 2024. Vol. 94. No. 7. pp. 786-804.
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Dikusar E. A., Akishina E. A., Zhukouskaya N. A., Kolesnik I. A., Margun E. N., Kovalskaya S. S., Alekseeva K. A., Logvinenko N. A., Menshikova D., Grigoriev M. S., I. Potkin V. Synthesis of Formylphenyl 1-Oxo-1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole-7-carboxylates and Their (E)-1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazole-4-yliminomethyl Derivatives // Журнал Общей Химии. 2024. Vol. 94. No. 7. pp. 786-804.
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TY - JOUR
DO - 10.31857/s0044460x24070016
UR - https://journals.rcsi.science/0044-460X/article/view/273626
TI - Synthesis of Formylphenyl 1-Oxo-1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole-7-carboxylates and Their (E)-1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazole-4-yliminomethyl Derivatives
T2 - Журнал Общей Химии
AU - Dikusar, E A
AU - Akishina, E A
AU - Zhukouskaya, N A
AU - Kolesnik, I A
AU - Margun, E. N.
AU - Kovalskaya, S. S.
AU - Alekseeva, K. A.
AU - Logvinenko, N. A.
AU - Menshikova, Daria
AU - Grigoriev, Mikhail S.
AU - I. Potkin, Vladimir
PY - 2024
DA - 2024/12/20
PB - The Russian Academy of Sciences
SP - 786-804
IS - 7
VL - 94
SN - 0044-460X
ER -
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@article{2024_Dikusar,
author = {E A Dikusar and E A Akishina and N A Zhukouskaya and I A Kolesnik and E. N. Margun and S. S. Kovalskaya and K. A. Alekseeva and N. A. Logvinenko and Daria Menshikova and Mikhail S. Grigoriev and Vladimir I. Potkin},
title = {Synthesis of Formylphenyl 1-Oxo-1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole-7-carboxylates and Their (E)-1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazole-4-yliminomethyl Derivatives},
journal = {Журнал Общей Химии},
year = {2024},
volume = {94},
publisher = {The Russian Academy of Sciences},
month = {dec},
url = {https://journals.rcsi.science/0044-460X/article/view/273626},
number = {7},
pages = {786--804},
doi = {10.31857/s0044460x24070016}
}
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MLA
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Dikusar, E. A., et al. “Synthesis of Formylphenyl 1-Oxo-1,2,3,6,7,7a-hexahydro-3a,6-epoxyisoindole-7-carboxylates and Their (E)-1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazole-4-yliminomethyl Derivatives.” Журнал Общей Химии, vol. 94, no. 7, Dec. 2024, pp. 786-804. https://journals.rcsi.science/0044-460X/article/view/273626.