Open Access

MolBank, volume 2023, issue 1, pages M1565

5-Vinyl-1H-tetrazole

Daria M. Krygina ¹

Eugene V. Sivtsov ²

Yuliya N. Pavlyukova ³

E. N. Chernova ⁴

Mariya A. Skryl’nikova ^{3, 5}

Vadim A. Baigildin ⁶

Aleksandra M. Puzyk ⁷

Alexander A. Oskorbyn ²

Rostislav E. Trifonov ³

Pavel A. Aleshunin ³

Vladimir A. Ostrovskii ^{3, 4}

Hide authors affiliations Show authors affiliations: 7 affiliations

Laboratory of Polymer Sorbents and Carriers for Biotechnology, Institute of Macromolecular Compounds, Russian Academy of Sciences (IMC RAS), 31 Bolshoy Prospekt V.O., 199004 St. Petersburg, Russia |

Department of Physical Chemistry, Saint Petersburg State Institute of Technology, 24–26/49 Moskovsky Ave., 190013 St. Petersburg, Russia |

Department of Chemistry and Technology of Nitrogen-Containing Organic Compounds, Saint Petersburg State Institute of Technology, 24–26/49 Moskovsky Ave., 190013 St. Petersburg, Russia |

⁴

Saint Petersburg Federal Research Center, Russian Academy of Sciences (SPC RAS), 39, 14th Line, 199178 St. Petersburg, Russia |

⁵

Department of Organic Chemistry, Saint Petersburg State Institute of Technology, 24–26/49 Moskovsky Ave., 190013 St. Petersburg, Russia |

⁶

Department of General and Inorganic Chemistry, Institute of Chemistry, Saint Petersburg State University, 26 Universitetskii Prospect, Petergof, 198504 St. Petersburg, Russia |

⁷

Research Park, Saint Petersburg State University, 26 Universitetskii Prospect, Petergof, 198504 St. Petersburg, Russia |

Publication type: Journal Article

Publication date: 2023-01-23

MDPI

Journal: MolBank

Quartile SCImago

Quartile WOS

SJR: 0.150

CiteScore: 0.7

Impact factor: 0.6

ISSN: 14228599

DOI: 10.3390/m1565

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Organic Chemistry

Biochemistry

Physical and Theoretical Chemistry

Abstract

Highly purified 5-vinyl-1H-tetrazole was synthesized, which is in great demand in modern medicine and industry as a monomer for obtaining nitrogen-rich macromolecular compounds and a reagent for the complete synthesis of biological compounds. The molecular structure was studied experimentally with sequential X-ray diffraction analysis and theoretically with ab initio quantum chemical calculations. The data from differential scanning calorimetry, nuclear magnetic resonance (1H, 13C, 1H-15N, HMBC), high-resolution mass spectrometry and vibrational spectroscopy were analyzed. The results are useful for evaluating the possibility of extending the polymerization of 5-vinyl-1H-tetrazole to synthesize polymers with predictable molecular weight and thermodynamic parameters.

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Krygina D. M. et al. 5-Vinyl-1H-tetrazole // MolBank. 2023. Vol. 2023. No. 1. p. M1565.

GOST all authors (up to 50) Copy

Krygina D. M., Sivtsov E. V., Pavlyukova Y. N., Chernova E. N., Skryl’nikova M. A., Baigildin V. A., Puzyk A. M., Oskorbyn A. A., Trifonov R. E., Aleshunin P. A., Ostrovskii V. A. 5-Vinyl-1H-tetrazole // MolBank. 2023. Vol. 2023. No. 1. p. M1565.

RIS |

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RIS Copy

TY - JOUR

DO - 10.3390/m1565

UR - https://doi.org/10.3390/m1565

TI - 5-Vinyl-1H-tetrazole

T2 - MolBank

AU - Krygina, Daria M.

AU - Sivtsov, Eugene V.

AU - Pavlyukova, Yuliya N.

AU - Chernova, E. N.

AU - Skryl’nikova, Mariya A.

AU - Baigildin, Vadim A.

AU - Puzyk, Aleksandra M.

AU - Oskorbyn, Alexander A.

AU - Trifonov, Rostislav E.

AU - Aleshunin, Pavel A.

AU - Ostrovskii, Vladimir A.

PY - 2023

DA - 2023/01/23

PB - MDPI

SP - M1565

IS - 1

VL - 2023

SN - 1422-8599

ER -

BibTex |

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BibTex Copy

@article{2023_Krygina,

author = {Daria M. Krygina and Eugene V. Sivtsov and Yuliya N. Pavlyukova and E. N. Chernova and Mariya A. Skryl’nikova and Vadim A. Baigildin and Aleksandra M. Puzyk and Alexander A. Oskorbyn and Rostislav E. Trifonov and Pavel A. Aleshunin and Vladimir A. Ostrovskii},

title = {5-Vinyl-1H-tetrazole},

journal = {MolBank},

year = {2023},

volume = {2023},

publisher = {MDPI},

month = {jan},

url = {https://doi.org/10.3390/m1565},

number = {1},

pages = {M1565},

doi = {10.3390/m1565}

}

MLA

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MLA Copy

Krygina, Daria M., et al. “5-Vinyl-1H-tetrazole.” MolBank, vol. 2023, no. 1, Jan. 2023, p. M1565. https://doi.org/10.3390/m1565.

Found error?

Publisher

MDPI

Journal

MolBank

Quartile SCImago

Quartile WOS

SJR

0.150

CiteScore

0.7

Impact factor

0.6

ISSN

14228599 (Print, Electronic)

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