Open Access
Polymers, volume 15, issue 8, pages 1896
Advanced Electrode Coatings Based on Poly-N-Phenylanthranilic Acid Composites with Reduced Graphene Oxide for Supercapacitors
Tkachenko Lyudmila Ivanovna
2
,
Efimov Oleg Nikolaevich
2
,
Nikolaeva Galina Vasilevna
2
,
Kostev Aleksandr Ivanovich
1
,
Dremova Nadejda Nikolaevna
2
,
Publication type: Journal Article
Publication date: 2023-04-15
General Chemistry
Polymers and Plastics
Abstract
The electrochemical behavior of new electrode materials based on poly-N-phenylanthranilic acid (P-N-PAA) composites with reduced graphene oxide (RGO) was studied for the first time. Two methods of obtaining RGO/P-N-PAA composites were suggested. Hybrid materials were synthesized via in situ oxidative polymerization of N-phenylanthranilic acid (N-PAA) in the presence of graphene oxide (GO) (RGO/P-N-PAA-1), as well as from a P-N-PAA solution in DMF containing GO (RGO/P-N-PAA-2). GO post-reduction in the RGO/P-N-PAA composites was carried out under IR heating. Hybrid electrodes are electroactive layers of RGO/P-N-PAA composites stable suspensions in formic acid (FA) deposited on the glassy carbon (GC) and anodized graphite foil (AGF) surfaces. The roughened surface of the AGF flexible strips provides good adhesion of the electroactive coatings. Specific electrochemical capacitances of AGF-based electrodes depend on the method for the production of electroactive coatings and reach 268, 184, 111 F∙g−1 (RGO/P-N-PAA-1) and 407, 321, 255 F∙g−1 (RGO/P-N-PAA-2.1) at 0.5, 1.5, 3.0 mA·cm−2 in an aprotic electrolyte. Specific weight capacitance values of IR-heated composite coatings decrease as compared to capacitance values of primer coatings and amount to 216, 145, 78 F∙g−1 (RGO/P-N-PAA-1IR) and 377, 291, 200 F∙g−1 (RGO/P-N-PAA-2.1IR). With a decrease in the weight of the applied coating, the specific electrochemical capacitance of the electrodes increases to 752, 524, 329 F∙g−1 (AGF/RGO/P-N-PAA-2.1) and 691, 455, 255 F∙g−1 (AGF/RGO/P-N-PAA-1IR).
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Ozkan S. Z. et al. Advanced Electrode Coatings Based on Poly-N-Phenylanthranilic Acid Composites with Reduced Graphene Oxide for Supercapacitors // Polymers. 2023. Vol. 15. No. 8. p. 1896.
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Ozkan S. Z., Tkachenko L. I., Efimov O. N., Karpacheva G., Nikolaeva G. V., Kostev A. I., Dremova N. N., Kabachkov E. N. Advanced Electrode Coatings Based on Poly-N-Phenylanthranilic Acid Composites with Reduced Graphene Oxide for Supercapacitors // Polymers. 2023. Vol. 15. No. 8. p. 1896.
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TY - JOUR
DO - 10.3390/polym15081896
UR - https://doi.org/10.3390%2Fpolym15081896
TI - Advanced Electrode Coatings Based on Poly-N-Phenylanthranilic Acid Composites with Reduced Graphene Oxide for Supercapacitors
T2 - Polymers
AU - Ozkan, Sveta Zhiraslanovna
AU - Tkachenko, Lyudmila Ivanovna
AU - Efimov, Oleg Nikolaevich
AU - Karpacheva, Galina
AU - Nikolaeva, Galina Vasilevna
AU - Kostev, Aleksandr Ivanovich
AU - Dremova, Nadejda Nikolaevna
AU - Kabachkov, Eugene N
PY - 2023
DA - 2023/04/15 00:00:00
PB - Multidisciplinary Digital Publishing Institute (MDPI)
SP - 1896
IS - 8
VL - 15
SN - 2073-4360
ER -
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@article{2023_Ozkan,
author = {Sveta Zhiraslanovna Ozkan and Lyudmila Ivanovna Tkachenko and Oleg Nikolaevich Efimov and Galina Karpacheva and Galina Vasilevna Nikolaeva and Aleksandr Ivanovich Kostev and Nadejda Nikolaevna Dremova and Eugene N Kabachkov},
title = {Advanced Electrode Coatings Based on Poly-N-Phenylanthranilic Acid Composites with Reduced Graphene Oxide for Supercapacitors},
journal = {Polymers},
year = {2023},
volume = {15},
publisher = {Multidisciplinary Digital Publishing Institute (MDPI)},
month = {apr},
url = {https://doi.org/10.3390%2Fpolym15081896},
number = {8},
pages = {1896},
doi = {10.3390/polym15081896}
}
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Ozkan, Sveta Zhiraslanovna, et al. “Advanced Electrode Coatings Based on Poly-N-Phenylanthranilic Acid Composites with Reduced Graphene Oxide for Supercapacitors.” Polymers, vol. 15, no. 8, Apr. 2023, p. 1896. https://doi.org/10.3390%2Fpolym15081896.